碳量子点的制备与介绍.ppt

The carbon dots were reported as potential candidates to replace heavy metal QDs,especially for biological applications. The synthesis of carbon dots mainly consists of three steps： synthesis of raw carbon dots, surface passivation and functionalization. Raw carbon dots are synthesized by top down and bottom up approaches. Top down method includes arc-discharge,laser ablation and several electrochemichal methods,while bottom up approach includes the methods like thermal carbonization of carbon precursors,acid dehydration of carbohydrates，heating by microwave or ultrasonic treatment of acidified carbon sources. 2.Synthetic methods 3.Results and Discussion * Ascorbic Acid Assisted Green Route for Synthesis of Water Dispersible Carbon Dots 孔文瀚 201341603030 1、Introduction 2、Experimental 2.1 Materials 2.2 Synthesis Method 2.3 Characterization 3、Future target Content 1.Introduction Carbon quantum dots (CQDs) are a new class of quantum dots materials Inorganic quantum dots Carbon quantum dots Ref. 1 Youfu Wang, Aiguo Hu. J. Mater. Chem. C, 2014, 2, 6921–6939 2 Shi Ying Lim, Wei Shen and Zhiqiang Gao, Chem. Soc. Rew., 2015, 362-281 2.Experimenta 2.1 Materials Ascorbic acid(99％)，phenol and 2-aminophenol were purchased from Tianjin Guangfu Chemical Co，China． L-Lysine(99％) was purchased from Dingguo Corporation， Shanghai，China．All other reagents were of analytical grade and used without further purification． Many methods have been proposed to prepare CQDs during the last decade, which can be roughly classified into “Top-down” and “Bottom-up” approaches. 146 mg(1 mm01)of L-lysine and 176 mg(1 mm01)of ascorbic acid were dissolved in 20 mL of distilled H，O and stirred for l h．Then the solution was transferred to an autoclave for further condensation at 140。C for 12 h．Finally,the carbon dot solution was obtained after centrifugation to remove the suspended particles，then the sample was dialyzed for 24 h to remove the organic funct