与食品接触的塑料成型品中邻苯二甲酸酯类增塑剂迁移量的测定_孙利.pdfVIP

2008 3 18 3 Ch inese Journal ofH ea lth Laboratory Te hnology, M ar 2008; Vol 18 No 3 393 与食品接触的塑料成型品中邻苯二甲酸酯类增塑剂迁移量的测定 * 孙利, 陈志锋 , 雍伟, 储晓刚 ( , 100025) [ ] : : ( 3% 10% ), : 4, 800% ~ 1080% , 747: , [ ] 食品接触材料; 塑料成型品; 邻苯二甲酸酯; 特定迁移量 [ ] O65763 [] A [] 1004- 8685( 2008) 03- 0393- 04 D eterm ination of m igration of phthalates in p lastic articles in tended to com e in to con tact w ith food stuffs- GC /M S * S un L i, Chen Zh i-f eng , Yong W e,i Ch u X iao-g ang ( ChineseA adem y of Inspe tion and Quarantine, Beijing 100025, Ch ina) [ Ab stract] O bjective To establish a new m ethod for determ ination of phthalates from p lasti arti les in food smi u lants by GC / M SM ethods The aqueous smi ulan t ( d istilled w ater, 3% (w / v) a eti a id aqueous solution, 10% ( v/v) ethanol aqueous so- lution) test sam ples were extra ted w ith n- hex ane and isoo tane was d ilu ted by n- hex ane for inje tion d ire tlyR esu lts In fou r smi u lants, the rate of re overy was bewt een 800% and 1080% andR SD less than the referen e value 747Conc lu sion This m ethod has good sensitivity, a ura y, repeatab ilityThe lmi it of quantitation of this m ethod an m eet the in ternational standard [ K ey words] Food onta tm aterial; Plasti arti le; phthalates; Spe ial m igration , , [4, 5] , , , , , , 1 11 试 与仪器 [ 1] ,