bibw2992阿法盐的LCMS.pdfVIP

LC/MS Report Injection Date : 14 Mar 14 1:12 pm +0800 Tgt Mass(EZX) : Acq. Operator : LCMSA043 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : C:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : C:\Chem32\1\METHODS\1-POS-3MIN.M Sample Info : *** No target masses specified *** Method Info : Mobile Phase: A: water(10mM Ammonium hydrogen carbonate) B: ACN Gradient: 5%-95% B in 1.5min Flow Rate: 2.0ml/min Column: XBridge C18,4.6*50mm,3.5um Oven Temperature: 40 C MASS Range:110-800 *ELS 1 A , Voltage mV 100 75 50 25 0.5 1 1.5 2 2.5 3 min* *DA D1 A , Sig=214,4 Ref =off mAU 6 2 9 . 400 1 200 0 0.5 1