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Low-temperature synthesis of δ-MnO2 with large surface area and its capacitance
Materials Letters 64 (2010) 1763–1765
Contents lists available at ScienceDirect
Materials Letters
journa l homepage: /locate/matlet
Low-temperature synthesis of δ-MnO2 with large surface area and its capacitance
Gang Zhu, Hongjuan Li, Lingjuan Deng, Zong-Huai Liu ⁎
Key Laboratory of Applied Surface and Colloid Chemistry (Shaanxi Normal University), Ministry of Education, Xian, 710062, PR China; School of Chemistry and Materials Science,
Shaanxi Normal University, Xian, 710062, PR China
a r t i c l e i n f o a b s t r a c t
Article history: δ-MnO2 was synthesized by a facile low-temperature hydrothermal method with a mixed system of KMnO4
Received 5 February 2010 and CO(NH ) at 90 °C for 24 h. The obtained product was characterized by X-ray diffraction (XRD), scanning
2 2
Accepted 14 May 2010 electron microscopy (SEM) and N2 adsorption–desorption. Results showed that the as-synthesized product
Available online 24 May 2010 2 − 1
had a layered structure and a high specific surface area of 230 m g . Electrochemical characterization
indicated that the prepared material exhibited an ideal capacitive behavior with the initial capacitance value
Keywords: − 1 − 1
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