Low-temperature synthesis of δ-MnO2 with large surface area and its capacitance.pdf

Low-temperature synthesis of δ-MnO2 with large surface area and its capacitance.pdf

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Low-temperature synthesis of δ-MnO2 with large surface area and its capacitance

Materials Letters 64 (2010) 1763–1765 Contents lists available at ScienceDirect Materials Letters journa l homepage: /locate/matlet Low-temperature synthesis of δ-MnO2 with large surface area and its capacitance Gang Zhu, Hongjuan Li, Lingjuan Deng, Zong-Huai Liu ⁎ Key Laboratory of Applied Surface and Colloid Chemistry (Shaanxi Normal University), Ministry of Education, Xian, 710062, PR China; School of Chemistry and Materials Science, Shaanxi Normal University, Xian, 710062, PR China a r t i c l e i n f o a b s t r a c t Article history: δ-MnO2 was synthesized by a facile low-temperature hydrothermal method with a mixed system of KMnO4 Received 5 February 2010 and CO(NH ) at 90 °C for 24 h. The obtained product was characterized by X-ray diffraction (XRD), scanning 2 2 Accepted 14 May 2010 electron microscopy (SEM) and N2 adsorption–desorption. Results showed that the as-synthesized product Available online 24 May 2010 2 − 1 had a layered structure and a high specific surface area of 230 m g . Electrochemical characterization indicated that the prepared material exhibited an ideal capacitive behavior with the initial capacitance value Keywords: − 1 − 1

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