金银花醇沉多阶段多变量统计过程控制研究介绍.PDF

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金银花醇沉多阶段多变量统计过程控制研究介绍.PDF

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• 784 • ( ) JTCMP , April 2012, Vol . 27, No. 4 Multi-phase and multivariate statistical process control for alcohol precipitation of water extract of Lonicerae Japonicae XU Bing, SHI Xin-yuan, QIAO Yan-jiang, DU Min, SUI Cheng-lin, LIU Qian ( School of Chinese Pharmacy, Beijing University of Chinese Medicine, Beijing 100102, China ) Abstract: Objective: To establish the multi-phase and multivariate statistical process control strategy for alcohol precipitation of water extract of Lonicerae Japonicae . Methods: Based on the concept of PAT, NIR technology was applied to monitor the alcohol precipitation process in real time. Then the process was divided into several phases by sequential clustering 2 analysis using the process NIR spectra. The MSPC models as well as the Hotelling T and SPE control limits were built for the whole process and each phases.The effects of the whole process MSPC model and phase based MPSC model were compared. Results: Alcohol