大尺度n is 纳米线的超声喷雾热解制备 - 工程技术版.pdf

8 2 () Vo.l 8 No. 2 2008 6 JOURNAL OF NAN JING NORMAL UN IVERSITY ( ENG INEERING AND TECHNOLOGY EDIT ION ) Jun, 2008 大尺度 N iS 纳米线的超声喷雾热解制备 2 申秋芳, 周晓锋, 王声乐 (, 211189) [ ] N iC l 6H O, 350, , 2 2 . X ( XRD)( TEM ) . : N iS ( 200), 25: 1, 2 . [ ] N iS , , , 2 [ ] TB383 [] B [ ] 1672-1292( 2008) 02-0059-03 Syn thesis of L arge-scale N i S Nanow ires by U ltrason ic Spray Pyrolysis M ethod 2 Shen Q iufang, Z hou X iao feng, W ang S hengyue ( D partm nt of Physics, South astU n iv rsity, N anjing 211189, Ch ina) A bstrac t: Larg -scal nanow ir s of N iS w r synth siz d using N iC l6H O and th iour a ( CS( NH ) ) as r actant by 2 2 2 2 2 an ultrasonic spray pyrolysis t chniqu comb in ing w ith soft-t mp lat on glass substrat at 350 . Th pr par d sam pl s w r charact riz d by using XRD, TEM and opticalm icroscop . Th r su lts show that th s larg -scal nanow ir s w r N iS nanow ir s w ith( 200) pr f r ntial grow th and diam t r and l ngth ratio of 251. Its grow th m chan ism w as pr lmi i- 2 narily d iscuss d as w ll. K ey w ord s: N iS , nanow ir s, ultrason ic spray pyroly sis, soft-t m plat 2 MX 2 (M = M n, F , Co, N i; X = S, S , T ) , . [ 1, 2] , , . [ 3] [ 4] [ 5] , [ 6] [ 7 ]