AMA254汞分析仪测定颗粒物中痕量总汞的研究.pdfVIP

中国环场监测 Vol. 25 No.4 第 25 卷第4 期 2创19 年 8 月 Environmental Monitoring in China Aug.2αm AMA254 宋分析仪测定颗粒物中痕量总隶的研究 2 何 灿1 ，高良敏l ，汪桂林1 ，程学丰l ，张明旭1 ， Wei-Pi吨 Pan (1.安徽理工大学地球与环堤学院，安徽淮南 232ω1 ; 2. Institute for combustion Science and Technology , West Kentucky University , Bowling Green , KY 4210 1, USA) 摘 要:采用 AMA254 杀分析仪测定大气颗粮物和煤中的痕f总朵，建立了或接测定颗靠在物中痕f总泉的分析方法。测 l 定结果农明，在采绝对含受沟。-35ng 范周内线性良好，测定大气颗粒物和煤中的痕爱总杀的扮出限分别为 O.06ng/m 和 0.02鸣句，标准样品测定的 RSD.s;;; 0.78% ，加栋回收率为 929品制 1089品 。该方法具有无需消解11接进样测定、极其简便、 省时等特点，适合多种阂体样品中痕受系的测定。 关键词:系; AMA254; 大气颗糕物:煤 中图分类号: X831 文献标识码:A 文章编号:1 ∞2翩翩2(2棚)04耐26耐 Study OD Detennination or Trace Mercury 旭 with AMA254 Mercury Analyzer 1 日应 Can , et aI (1. SchoolQf 且z由 and Environment , Anhui Uníversíty of Scíence and Technology , Huainan 232001 , Chína) Abstract : A novel method for determination of vace 川ercury ín particulate matter by AMA2 54 Mercl町 Analyzer wi由 direct samplíng was establíshed. The results shoWed the good línearity wωachieved in the rang from Ong to 35ng of ωtaI mercury absolute content , the detection límít of atm08phefÍc particulate and coal were O. O6ngl旷和 O.02nglg se阴rately ， RSD of standard sample E 0.78 % , recoveries were between 92 9串 -108% .响le experiment results show that the 翩翩y was with hígh 阴阳ítivíty ， stabγlíty 朋d 盹lectívíty. The