DSC 热分析仪培训资料.pptVIP

DSC６２００ DSC Basics Basic Training Outline Theory/Design (Basic) Installation Installation Procedures Hardware Software Basic Accessories Operation Calibration Troubleshooting DSC (Differential Scanning Calorimetry) A thermal analysis technique which monitors/measures the energy absorbed or liberated from a material as it is subjected to a temperature profile Isothermal or programmed heat/cool All Seiko DSC’s are heat flux instruments where the ΔT between the sample and reference is measured and converted to energy units Sample TC Reference TC Control TC Conventions Endotherms down Sample on right SII Nanotechnology DSC Operation Theory DSC Components Heater Furnace and windings Control thermocouple Temperature Sensor Senses temperature Sample thermocouple Reference thermocouple Heat Sink Cover Insulating Cover DSC DSC6200 Two configurations Standard Ships with MUSE F/W Autosampler (ASD-2) Ships with MUSE F/W Installation Connect cables Connect purge gas Connect peripheries Install and align AS (if applicable) Connect computer components Install Muse/Exstar Perform installation protocol checks Signoff DSC Interconnects DSC with Autosampler DSC Measurement Cell Models DSC6200 Oval Sensor Constantan disk Silver disk Chromel/Alumel TC DSC Sensor (Oval Sensor) Purge gas inlet Sample TC ~ 7.8 ohms Reference TC Combines with Sample ~ 12.0 ohms Control (Furnace) TC ~ 10.6 ohms Heater ~ 54.4 ohms DSC Measurement Head Electronics DSC Furnace DSC6200/DSC (Sensor Constantan) Temperature Range: -150 to 725 oC Measurement Range (Sensitivity): +/- 100 mW (0.4 μW) Auto Cooling Accessory (LN2) Electrical Cooling (Refrigeration Unit) Auto Air Cooling (Gas Cooling) DSC Base Unit Electronics ASD-2 Installation Install ASD-2 on top of DSC Secure with mounting bracket Align front to back using string Tighten bracket Align AS positions ASD-2 “Adjusting the Transport System” Place sample pan on tray (Position 1) Place Inner Lid and Outer Lid onto their respective sta