液相法合成纳米金属氧化物晶体.PDF

53 Solution Method for Synthesizing Nanocrystal of Metal Oxide ,,, , ( , 550003) ZHAN Xue-jun, FU L-i ye, ZHAN Meng-meng, LIU Peng, UO Zhi-hui ( uizhou Province Key Laboratory of Fermentation Engineering Biological Pharmacy, uizhou University, uiyang 550003, China) : (-) , X , , : ; ;; ; : TB34 : A : 1001-4381( 2008) 10-0053-07 Abstract: T he solution method, such as the so-l gel process,could directly synthesize nano-scale metal oxide crystal and dope nano-scale metal oxide crystal under assistance of anion-exchange resin and or- ganic solvent. The synthesized nano-scale crystals were dried through the azeotropic distillation using iso-amyl acetate as azeotropic solvent and a highly dispersed powder was obtained. T he analysis that conducted on transmission electron microscope (T EM) and X-ray diffractometer (XRD) demonstrated the nano-scale powder did possess distinctly crystalline structure, and showed a high photo-catalysis and ant-i bacterial that only crystal had. Key words: solution method;anion-exchange resin;organic solvent; azeotropic drying;nanocrystal - - - OH ( Cl , NO3 ) , , , ( ) , , , , , () , , , , () , ( 300e ) , , 1