火焰原子吸收光谱法测定地奥明七硫酸酯钠中钠的含量-中国药事.PDF

2008 223 233 岳志华, 金红宇, 张启明( , 100050) : 建立火焰原子吸收光谱法测定地奥明七硫酸酯钠中钠含量的方法采用标准曲 法, 钠浓度在 06~ 14mg 1 标准曲 范围内 性良好, 相关系数为09991, 加样回收率为1003% , RSD 为09% 1 结果6 份样品测得钠的平均含量为01461mg mg , RSD 为08%实验结果表明, 本法精密度高, 准确性和重现性好, 可用于控制地奥明七硫酸酯钠中钠的含量 : 火焰原子吸收光谱法; 钠; 地奥明七硫酸酯钠 : R9272 : A :(2008) Determination of Sodium in Diosmin Heptakis Hydrogensulfate Sodiumby FAAS Yue Zhihua, Jin Hongyu and Zhang Qiming ( National Institute for the Control of Pharmaceutical and Biological Products, Beijing 100050) ABSTRACT T o establish a FAAS method to determine sodium in diosmin heptakis hydrogensulfate sodium. T he good linearity was obtained when the concentration of sodium was within the range of 06~ 1 14mg , the correlation coefficient is 09991. T he recovery ratio by standard addition is 1003%, and 1 RSD is 09%. T he content of sodium in diosmin heptakis hydrogensulfate sodium is 01461mg mg . The method is accurate with a good precision and reproduction. KEY W RDS flame atomic absorption spectrophotometry; sodium; diosmin heptakis hydrogensulfate sodium , , 12 KBr , KBr 1525g, 100m , , , 05%KBr , , 13 1 KBr 10m 50m , ( , , , 2 ; KBr, M6 , Na 1000g m 1 ( ( ) ; : ) : 8mA ; : 5890nm; : 11 02nm; : 70mm ; 1000g m 1 ; : 40s; : ( ) 1m 100m , 3 , , 10g m 1 31 : , , ; Tel: ( 010) E- mail: zhihuaamt@ 163. com 234 2008 2