食品中塑化剂的检测（SPE-GCMS,LCMS）.PDFVIP

SPE-GC/MS,LC/MS QueChERS ( 60105204) GC/MS 1. 5.0g TG-5MS 30m0.25mm0.25µm 25mL 10mL 6g MgSO4 1.5g Thermo 26098-1420 QueChERSPN:60105-341 1min4000r/min 2min40 5mL 60 1min 15 /min 2. 230 1min5 /min 280 4min 5.0g 50mL 5mL 1mL/min 15mL 6g MgSO4 1.5g Thermo QueChERSPN:60105-341 1min4000r/min 10µL 2min40 5mL 50mg PSA 50mg C18 150mg MgSO4 Thermo QueChERS clean-upPN:60105-204 250 1min4000r/min 2min 0.8min 50mL/min MS GC/MS 1. 25ppb 16 2. 45 LC/MS Thermo AccuCore RP-MS 2.6m100mm2.1mm 17126-102130 A: B: (min ) A: B: 0 60% 40% 12 0 100% 15 0 100% 0.3mL/min 3µL MS ESI SRM 3700V 350 1.22 2. 80-120% 46