低温球磨装置.PDFVIP

低温球磨装置 低温球磨装置 一、设备简介 自制非标设备，用于多种类型材料的粉碎或机械合金化。 二、 主要性能指标及具体参数 1. 容积：30 L 。 2. 工作温度：+30 ℃—-160℃。 3. 工作真空度：100 Pa。 4. 变频调速，输出转速 n ≤ 200 r/min 。 5. 低温球磨时可在线检测球磨温度，自动记录球磨机工作时的各项性能参 数（如转速、扭矩、温度等），并以电子文件的形式保存。 Cryogenic reaction attritor milling, or cryomilling, is a high energy ball milling process, by which elemental and pre-alloyed powders are milled in cryogenic media, e.g. liquid nitrogen, liquid argon, etc., to form a slurry. So far, most of the cryomilling has been carried out in liquid nitrogen. It has been suggested that the presence of liquid nitrogen during milling prevents problems induced by heating during milling and leads more rapidly to a smaller crystallite size. Advantages of Using the Attritor: Fast and efficient grinding Numerous options Flexibility Repeatability Easy operation Low maintenance Common Applicatons for the Attritor: Metal powders Metal oxides Glasses Minerals, coal Chemicals Food products …… 三、 设备照片、现场使用照片 图1低温球磨装置 四、 教学和科研工作的成果 图2 120 K 低温球磨 10 h 后纳米 Al-Zn-Mg-Cu 合金粉的 TEM 像 Fig.2 TEM photograph of Al-Zn-Mg-Cu alloy powders versus milling time at 120K for 10 h 110 100 ( 1 1 1 ) ) m 90 n ( 80 e z 70 i s n 60 i a r 50 G 40 30 0 2 4 6 8 10 Cryomilling time (h) 图3 Al-Zn-Mg-Cu 合金粉平均晶粒尺寸随球磨时间的变化情况 Fig.3 The grain size of Al-Zn-Mg-Cu alloy powders versus milling time at 120K in a