银_聚酰亚胺纳米复合颗粒的制备与性能表征.pdfVIP

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银_聚酰亚胺纳米复合颗粒的制备与性能表征.pdf

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银_聚酰亚胺纳米复合颗粒的制备与性能表征

19 4 2014 8 Vol.19 No.4 Materials Science and Engineering of Powder Metallurgy Aug. 2014 ( 410083) PAA(poly(amide acid))Ag PAA Ag/PAA PAA PI (polyimide) Ag/PI Ag PI PI Ag/PI TQ316.6+2 A 1673-0224(2014)4-0641-06 Preparation and characterization of silver/polyimide nanocomposite particles WANG Ya, LI Jun, WEN Jie-bin, CHEN Jun, CHEN Jiang-cong, LI Heng-feng (School of Materials Science and Engineering, Central South University, Changsha 410083, China) Abstract: Due to macromolecular coil-like structure of PAA (poly(amide acid)) and the interaction between PAA molecules and silver nanoparticles, the Ag/PI (polyimide) composite nanoparticles were in-situ prepared by chemical imidization of Ag/PAA solution. The morphology, thermal and dielectric properties of Ag/PI composite particles were investigated by transmission electron microscope, thermal analysis, Fourier transform infrared spectroscopy, and so on. The results show that silver nanoparticles were disperse uniformly in the PI matrix without serious migration and agglomeration even after certain thermal treatment. There are obvious interfacial polarization responses in the Ag/PI nanocomposite systems. It is the first time to try an all-in-situ method to prepare highly silver-doped PI nanocomposites. This experiment may provide a reference for the fabrication of high-performance Ag/PI dielectric nanocomposites in the future. Key words: poly(amic acid); polyimide; silver nanoparticles; chemical imidization; characterization