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ZnS@CdTe 包裹参考文献
FULL?PAPERDOI:10.1002/ejic.201201372Synthesis?of?Functionalized?Core–Shell?CdTe/ZnSNanoparticles?and?Their?Application?as?a?FluorescenceProbe?for?Norfloxacin?DeterminationLi?Li,*[a]?Yu?Cheng,[a]?Yaping?Ding,*[a]?Shuqing?Gu,[a]Fenfen?Zhang,[a]?and?Weijun?Yu[b]Keywords:?Nanoparticles?/?Cadmium?/?Zinc?/?Fluorescence?probesA?novel?and?simple?fluorometry?method?has?been?developedand?validated?for?the?determination?of?norfloxacin?(NOR)?onthe?basis?of?the?fluorescence?quenching?of?thioglycolic?acid(TGA)-capped?CdTe/ZnS?nanoparticles?(NPs)?by?NOR.?Thefunctionalized?CdTe/ZnS?NPs?were?successfully?synthesizedin?aqueous?medium?with?TGA?as?the?capping?ligand.?TGA-capped?CdTe/ZnS?NPs?were?characterized?by?using?X-raydiffraction?(XRD),?transmission?electron?microscopy?(TEM),particle?size?measurements,?and?Fourier?transform?infraredIntroductionNorfloxacin?(NOR),?a?widely?used?pharmaceutical?thatbelongs?to?the?second?generation?of?fluoroquinolones,?ischemically?named?1-ethyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazin-1-yl)?quinoline-3-carboxylic?acid.?It?is?consideredto?be?the?first?commercially?available?member?of?the?mod-ern?fluoroquinolones?and?has?seen?applications?in?the?ther-apy?of?gastrointestinal,?urinary,?and?respiratory?tract?infec-tions,?ocular?and?skin?infections,?as?well?as?in?patients?withintraabdominal?infections?in?combination?with?antianaero-bic?agents.[1–3]?In?recent?years,?NOR?has?been?ranked?as?thesecond-most-prescribed?fluoroquinolone?antibacterial?justnext?to?levofloxacin?in?China.[4]?It?is?clear?that?the?determi-nation?of?NOR?is?of?great?importance?on?account?of?thewidespread?use?of?NOR,?and?because?it?is?valuable?whenadjusting?the?drug?dosage.To?date,?numerous?methods?have?been?reported?for?theassay?of?NOR?in?pharmaceutical?preparations?or?biologicalsamples.?They?mainly?include?high-performance?liquidchromatography(HPLC),[5–8]?capillaryelectrophoresis(CE),[9–11]?spectrophotometry,[12,13]?and?electrochemicalanalysis.[4,14,15]?HPLC?and?CE?have?been?widely?used?
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