硫酸亚铁铵的制备（Preparation of ammonium ferrous sulfate）.docVIP

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硫酸亚铁铵的制备（Preparation of ammonium ferrous sulfate）.doc

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硫酸亚铁铵的制备（Preparation of ammonium ferrous sulfate） Purpose: Learn to prepare ammonium sulfate with differences in solubility; Master the properties of ferrous sulfate, ferrous sulfate and ammonium salt from the experiment; Master water bath, decompression, filtration and other basic operations; learn pH test paper, straw, color tube use; learning limit analysis; Through the calculation of feeding and the preparation of solution, the thinking and practice ability can be cultivated. Crystal size: Because the size of the precipitated crystal is related to the crystallization conditions, a suitable size crystal can be obtained by controlling the crystallization conditions. If the concentration of the solution is higher, the solubility of the solute is smaller, the cooling is faster, and the crystal solution is smaller when the stirring solution is not in use. On the contrary, if the concentration of the solution is not high, the cooling is slow, or a small crystal seed is placed, the larger crystal can be obtained. Principle hints: The preparation method of ferrous sulfate and ammonium ferrous sulfate is described. Write the response formula; Why can ammonium sulfate crystals be produced in the solution of ferrous sulfate and ammonium sulfate? Colorimetric principle. Step: 1g iron filings plus 5mL3mol L-1 sulfuric acid; In the fume hood, 353K the water bath is heated until the reaction is completed, and the total volume is maintained; Heat the filter; Unreacted iron filings were discarded; the amount of added (NH4) 2SO4 saturated solution in the filtrate was adjusted to pH = 1~2; Water bath is heated to crystallization film to cool and filter; Weighing crystals; discarding mother liquor. 2. limit analysis The oxygen free water preparation: Heat 150mL pure water until boiling in a 250mL cone, boil for 10~20 minutes at a low heat, cool and reserve. The sample solution preparation: 1g sample plus 2mL3mol, L-1HCl, 15mL, oxygen free water, oscillation, after the sample disso