过程控制剂对机械合金化Fe-48Al粉末特性的影响-材料工程.PDFVIP

60 / 2007 10 Fe-48Al Effects of Process Control Agents on Characteristics of Mechanically Alloyed Fe-48Al Powders ,, , ( , 100084) S NG Ha-i xia, WU Yun-xin, TANG Chuan-an, LIANG Ji (Department of Mechanical Engineering, T singhua University, Beijing 100084, China ) : ( PCA)-Fe-48Al( Al 48%, ) X , PCA ,Fe-48Al , ;PCA 12h , ; 1100 , FeAl( B ) , PCA Al 2 2 3 : ; FeAl; ;; : TG146 : A : 1001-4381(2007) 10-0060-05 Abstract: This paper dealt with the effects of process control agents ( PCA) , i. e., ethanol and stearic acid on the characteristics of mechanically alloyed Fe-48Al powders. T he particle size and particle morphology of the ball milled powders were investigated by means of laser mastersizer and scanning e- lectron microscope, and their microstructures were examined by X-ray diffractometer before and after heat treatment. The results indicate that, compared with stearic acid, ethanol facilitates faster me- chanical alloying of Fe-48Al, yielding much finer and more irregular plate-like powders. When using stearic acid as PCA, however, the milled powders tend to become thick plates or near-spherical part-i cles. T hemilled powders with either ethanol or stearic acid as PCA remain a solid solution structure e- ven after 12h milling, but both transform to FeAl (B2 ) intermetallic after subsequent vacuum annea- ling at 1100 , during which more Al2 3 is formed in the ethanol milled powders. Key words: process control agent; FeAl; mechanical alloying; heat treatment; powder FeAl , FeAl