物化讨论（Materialization discussion）.docVIP

物化讨论（Materialization discussion） Two, the device is convenient to study all kinds of liquids, such as benzene. Two vinyl chloride. Carbon tetrachloride. Water. Propanol. Isopropanol. Acetone and ethanol. Many of these liquids, flammable indeed, when heated, should pay attention to what the problem? Answer: heating, should slow heating, and careful control of temperature, the temperature of the solution can not exceed liquid fire, while a, C tube above the liquid level should not have air (or oxygen), besides the temperature gradually decreased by the way. The key to the experiment is that the successful ignition and the complete combustion of the sample are the key to the success of the experiment. The following technical measures can be considered: Sample should be grinded, dry, dryer, constant weight and other pre-treatment, wet sample is not easy to burn, and there is error. Compaction: generally hard to the surface, there is a relatively smooth finish, edges and corners without coarse particles, so that burning can not cause explosive combustion, residual black paste and so on. The ignition contact resistance wire and the electrode should be as small as possible, and pay attention to the problem of short circuit electrode loose wire glasses. Adequate oxygen (2MPa), and ensure oxygen bomb, do not leak oxygen, to ensure full combustion. Incomplete combustion, often shaped Become gray and white, such as loose cotton floc. Optical rotation Five. Think First, distilled water is used to correct the zero point of the polarimeter. In the process of sucrose conversion reaction, is it necessary to correct zero point t? Answer: sucrose solution uses distilled water as solvent, so pure distilled water is used as zero point correction. In the process of sucrose conversion, there is no need to make a zero point correction, because the distilled water is used as a correction, and only needs to be corrected once. Two. In the mixed sucrose solution and hydrochloric acid solution