超纯铁精矿粉直接还原制备超细铁粉 ultra-fine iron powder prepared by directly reducing super iron concentrates.pdfVIP

第 21 卷第 3 期 粉末冶金材料科学与工程 2016 年 6 月 Vol.21 No.3 Materials Science and Engineering of Powder Metallurgy Jun. 2016 超纯铁精矿粉直接还原制备超细铁粉 方建锋，郭培民，孔令兵，庞建明，赵志民 ( 中国钢研科技集团 新冶高科技集团有限公司，北京 100081) 摘要：将超纯铁精矿粉气流粉碎到微米级，用氢气直接还原制备超细铁粉，利用正交实验法研究还原温度、时间、 氢气流量等工艺参数对还原率的影响。结果表明：对超纯铁精矿粉还原率的影响程度从大到小依次为温度、时间、 氢气流量，综合考虑生产成本，确定最佳的还原工艺参数为温度 780 ℃、时间 60 min、氢气流量 0.3 L/min 。在此 工艺条件下得到的超细铁粉，全铁含量为 98.58%，氢损 0.45%，酸不溶物含量为 0.19%，其化学成分符合粉末冶 金用铁粉标准，一次粒度小于 5 μm 。 关键词：超纯铁精矿粉；直接还原；超细铁粉；正交试验；工艺参数；还原率 中图分类号：TF11 文献标志码：A 文章编号：1673−0224(2016)03−421−06 Ultra-fine iron powder prepared by directly reducing super iron concentrates FANG Jianfeng, GUO Peimin, KONG Lingbing, PANG Jianming, ZHAO Zhimin (Center of efficient utilization of resources by low-temperature metallurgy, China Iron Steel Research Institute Group, Beijing 100081, China) Abstract: The ultra fine iron powder was produced through directly reducing the super iron concentrates by H2, the super iron concentrates were milled into micrometer scale by jet mill machine before reducing. The effects of reducing temperature, time and flow rates of H2 on the reduction rate of super iron concentrates were studied by orthogonal experiments. The results show that the significantly descending order of parameters on the reduction rate is temperature, time and H2 flow rate. Considering the energy consumption, the optimal reducing parameters are 780 ℃ for 60 min with H2 flow rate of 0.3 L/min. The iron powder produced under these parameters has an Fe co