原创力文档an ef？cient synthesis of 1-aryl-3-(indole-3-yl)-3-(2-aryl-1,2,3-triazol-4-yl)propan-1-one catalyzed by a br？nsted acid ionic liquid英孚字母系数合成1-aryl-3 -(indole-3-yl)3(2-aryl-1 2 3-triazol-4-yl)propan-1-one催化br 望远镜酸离子液体.pdfVIP
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an ef？cient synthesis of 1-aryl-3-(indole-3-yl)-3-(2-aryl-1,2,3-triazol-4-yl)propan-1-one catalyzed by a br？nsted acid ionic liquid英孚字母系数合成1-aryl-3 -(indole-3-yl)3(2-aryl-1 2 3-triazol-4-yl)propan-1-one催化br 望远镜酸离子液体
Molecules 2010, 15, 9197-9204; doi:10.3390/molecule
OPEN ACCESS
molecules
ISSN 1420-3049
/journal/molecules
Article
An Efficient Synthesis of 1-Aryl-3-(indole-3-yl)-3-(2-aryl-1,2,3-
triazol-4-yl)propan-1-one Catalyzed by a Brønsted Acid
Ionic Liquid
Chen-Jiang Liu 1,2,* and Chuan-Ji Yu 2
1 Physics and Chemistry Detecting Center, Xinjiang University, 830046 Urumqi, China
2 Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education, School of Chemistry and
Chemical Engineering, Xinjiang University, 830046 Urumqi, China;
E-Mail: cjxyycj@126.com (C-J.Y.)
* Author to whom correspondence should be addressed; E-Mail: pxylcj@126.com;
Tel.: +86-991-8581211; Fax: +86-991-8582807.
Received: 11 October 2010; in revised form: 3 December 2010 / Accepted: 7 December 2010 /
Published: 10 December 2010
Abstract: An efficient synthesis of novel 1-aryl-3-(indole-3-yl)-3-(2-aryl-1,2,3-triazol-4-
yl)propan-1-ones from indoles and 1-aryl-3-(2-aryl-1,2,3-triazol-4-yl)propan-1-one using a
Brønsted acid ionic liquid [Sbmim][HSO ] as catalyst is described. Satisfactory results
4
with excellent yields and short reaction time were obtained in the experiments. The catalyst
could be recovered conveniently and reused efficiently.
Keywords: Brønsted acidic ionic liquid; Michael reaction; indoles; 1,2,3-triazole
Introduction
In recent years, β-indolylketones have received much attention because they represent an important
substructure in both biologically
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