gas chromatography the active paste menthol and methyl salicylate content（气相色谱活动粘贴薄荷醇,水杨酸甲酯内容）.docVIP

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gas chromatography the active paste menthol and methyl salicylate content（气相色谱活动粘贴薄荷醇,水杨酸甲酯内容）.doc

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gas chromatography the active paste menthol and methyl salicylate content（气相色谱活动粘贴薄荷醇,水杨酸甲酯内容）

Gas Chromatography the active paste menthol and methyl salicylate content [Abstract] Objective: To establish a the active cream active ingredients menthol and methyl salicylate capillary gas chromatographic method. Methods: chromatography conditions for PEG-20M capillary column 30 m × 0.25 mm × 0.25 μm, temperature program, starting temperature of 80 ° C to maintain elevated per minute after 5 min 15 ℃, the termination temperature of 190 ° C, held for 8 min, split ratio 50:1: each component in the corresponding concentration showed a good linear relationship, r1 = 0.999 79, r2 = 0.999 98, RSD ≤ 2.0%. Conclusions: The method is simple, rapid, accurate and can be used for quality control of the active paste. [Words] active cream; menthol; methyl salicylate Determination of the contents of mentholum and methyl salicylate in Medicated Balm by capillary gas chromatography MO Huodi, RONG Lingxin, HE Weirong, CHEN Guiping (The First Hospital of Zhaoqing City, Zhaoqing 526021, China) [Abstract] Objective: To establish a method for determination of the mentholum and methyl salicylate in Medicated Balm by capillary gas chromatography. Methods: Chromatographic condition was PEG-20M capillary column 30 m × 0.25 mm × 0.25 μm, initial temperature was 80 ℃, temperature programmed to raise 15 ℃ in five minutes, final temperature was 190 ℃ and kept eight minutes, split ratio was 50:1. Results: There was a favorable linearity relation between peak area and concentration. r1 = 0.999 79, r2 = 0.999 98 , RSD ≤ 2.0%. Conclusion: The method is sensitive, accurate and can be used for quality control of Medicated Balm. [Keywords:] Medicated Balm; Mentholum; Methyl salicylate The active cream “active oil” on the basis of the existing national drug standard varieties, keeping unchanged its original prescription, preparation process and route of administration, and further research trials to improve their formulations derived prescription by turpentine, camphor ,