化学类本科生毕业论文-《火焰原子吸收光谱法测定涂料中.docVIP

江苏科技大学本科毕业设计（论文） PAGE 26 江苏科技大学本科毕业论文 火焰原子吸收光谱法测定涂料中铅的含量 Sensitive Determination of lead by Flame Atomic Absorption Spectrometry 摘 要 本文简要介绍了涂料中存在的有毒有害物质以及国内外对其检测技术的现状。在实验中用溶剂将涂料离心分离得到颜料饼和萃取液，对这两部分进行处理后，采用火焰原子吸收法检测其中铅的含量。结果表明原子火焰吸收光谱法选择性较好，操作简便、准确度高，精确度好，能快速准确的检测出涂料中“可溶性”铅的含量。通过加标回收率的测定表明该方法测试灵敏度高、线性关系良好、分析准确。在对四种涂料分析检测后发现，其铅含量未超过国家标准，属于合格产品。 关键词：涂料的测定；铅的含量；火焰原子吸收光谱 Abstract This paper introduces the paint in the toxic and harmful substances, as well as domestic and foreign technology to detect the status quo. Solvents used in the experiment will be paint coating centrifuge cake and extract of the two parts processing, using FAAS detection of lead content. The results show that the flame atomic absorption spectrometry selective good, simple, high accuracy, precision, and can quickly and accurately detect the coating, soluble lead content. To increase the recovery of the test shows that the method of high sensitivity, linear relationship was good, accurate analysis. Four paint in the post-test analysis found that the lead content did not exceed national standards, are qualified products. Keywords: Paint determination; lead content; flame atomic absorption spectrometry 目 录 TOC \o \h \z \u HYPERLINK \l _Toc200872522 第一章 绪论 PAGEREF _Toc200872522 \h 1 HYPERLINK \l _Toc200872523 1.1引言 PAGEREF _Toc200872523 \h 1 HYPERLINK \l _Toc200872524 1.2我国涂料的现状 PAGEREF _Toc200872524 \h 1 HYPERLINK \l _Toc200872525 1.2.1我国涂料的主要种类 PAGEREF _Toc200872525 \h 1 HYPERLINK \l _Toc200872526 1.2.2 我国涂料工业的发展趋势 PAGEREF _Toc200872526 \h 2 HYPERLINK \l _Toc200872527 1.3涂料中有害物质介绍 PAGEREF _Toc200872527 \h 4 HYPERLINK \l _Toc200872528 1.3.1重金属 PAGEREF _Toc200872528 \h 4 HYPERLINK \l _Toc200872529 1.3.2甲醛 PAGEREF _Toc200872529 \h 4 HYPERLINK \l _Toc200872530 1.3.3苯系物 PAGEREF _Toc200872530 \h 4 HYPERLINK \l _Toc200872531 1.3.4 总挥发有机物（TVOC） PAGEREF _Toc200872531 \h 5 HYPERLINK \l _Toc200872532 1.3.5游离甲苯二异氰酸酯?(TDI?) PAGEREF _Toc200872532 \h 5 HYPERLINK \l _Toc200872533 1.3.6 氡