原创力文档synthesis of green-emitting (la,gd)obrtb3+ phosphors合成green-emitting(洛杉矶,gd)obrtb3 +荧光粉.pdfVIP
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synthesisofgreen-emitting(la,gd)obrtb3phosphors合成green-emitting(洛杉矶,gd)obrtb3荧光粉
Materials 2010, 3, 2506-2515; doi:10.3390/ma3042506
OPEN ACCESS
materials
ISSN 1996-1944
/journal/materials
Article
Synthesis of Green-Emitting (La,Gd)OBr:Tb3+ Phosphors
Sun Woog Kim, Kazuya Jyoko, Toshiyuki Masui and Nobuhito Imanaka *
Department of Applied Chemistry, Faculty of Engineering, Osaka University, 2-1 Yamadaoka, Suita,
Osaka 565-0871, Japan; E-Mails: swkim@chem.eng.osaka-u.ac.jp (S.W.K.);
kazuya@chem.eng.osaka-u.ac.jp (K.J.); masui@chem.eng.osaka-u.ac.jp (T.M.)
* Author to whom correspondence should be addressed; E-Mail: imanaka@chem.eng.osaka-u.ac.jp;
Tel.: +81-6-6879-7352; Fax: +81-6-6879-7354.
Received: 29 December 2009; in revised form: 12 March 2010 / Accepted: 31 March 2010 /
Published: 1 April 2010
Abstract: Green-emitting phosphors based on lanthanum-gadolinium oxybromide were
synthesized in a single phase form by the conventional solid state reaction method, and
photoluminescence properties of them were characterized. The excitation peak wavelength
of (La Gd )OBr:Tb3+ shifted to the shorter wavelength side with the increase in the
1-x x
crystal field around the Tb3+ ions by doping Gd3+ ions into the La3+ site, and, as a result,
the green emission intensity was successfully enhanced. The maximum emission intensity
was obtained for (La0.95Gd0.05)OBr:5%Tb3+, where the relative emission intensity was 45%
of that of a commercial green-emitting LaPO :Ce3+,Tb3+ phosphor.
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