载铂聚苯胺_聚砜复合膜修饰电极对甲醇的电催化氧化行为研究（Electrocatalytic oxidation of methanol on Pt PANI _ polysulfone composite membrane modified electrode）.docVIP

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载铂聚苯胺_聚砜复合膜修饰电极对甲醇的电催化氧化行为研究（Electrocatalytic oxidation of methanol on Pt PANI _ polysulfone composite membrane modified electrode）.doc

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载铂聚苯胺_聚砜复合膜修饰电极对甲醇的电催化氧化行为研究（Electrocatalytic oxidation of methanol on Pt PANI _ polysulfone composite membrane modified electrode）

载铂聚苯胺_聚砜复合膜修饰电极对甲醇的电催化氧化行为研究（Electrocatalytic oxidation of methanol on Pt PANI _ polysulfone composite membrane modified electrode） Thirty-eighth volume, fourth issue April 2009 Applied chemical Applied, Chem, ICA, l, Industry Vo.l 38 No. 4 Apr. 2009 Received date: 2009-02-07 revision date: 2009-02-23 Project supported by the key project of Baoji University of Arts and Sciences (ZK08118) Author: Ren Lijun (1981 -), female, Shaanxi Xingping, Baoji University of Arts and Sciences, master, mainly engaged in the research of electrode materials. Telephone: E - m, a, i:l, renlijun., W, ind@, com, 163. PT polyaniline / polysulfone composite membrane modified electrode Electrocatalytic oxidation of methanol Ren Lijun 1, Li Zongxiao 1, Hu in 2, Wang Xiaomei 1 (1. 、 Department of chemistry and chemical engineering, Baoji University of Arts and Sciences, Shaanxi 721013, China; 2.. School of chemistry and chemical engineering, Northwest Normal University, Gansu, Lanzhou, Baoji 730070) Abstract: polyaniline (PAN) / polysulfone (PSF) composite film modified electrode was prepared by cyclic voltammetry, and platinum nanoparticles were deposited on it to prepare platinum Polyaniline The electrocatalytic oxidation of methanol was studied by cyclic voltammetry and AC impedance with modified polysulfone composite membrane electrode. The chemical composition of the composite membrane is FTIR The surface morphology of the composite film after platinum loading was characterized by SEM. The results show that the inner layer of the composite film (one side of the contact with the working electrode) is The outer layer of polyaniline (contact with the solution) is polysulfone, and platinum particles are uniformly deposited on the porous polyaniline in the inner layer of the composite film, so as to make the platinum containing polyaniline / poly The composite electrode modified by sulfone composite has good electrocatalytic performance for methanol oxidation. Keywords: Pt loaded