氧化锌中铅、镉、汞的icp-oes法测定（Determination of lead, cadmium and mercury in Zinc Oxide by ICP-OES）.docVIP

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氧化锌中铅、镉、汞的icp-oes法测定（Determination of lead, cadmium and mercury in Zinc Oxide by ICP-OES）.doc

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氧化锌中铅、镉、汞的icp-oes法测定（Determination of lead, cadmium and mercury in Zinc Oxide by ICP-OES）

氧化锌中铅、镉、汞的icp-oes法测定（Determination of lead, cadmium and mercury in Zinc Oxide by ICP-OES） Determination of lead, cadmium and mercury in Zinc Oxide by ICP-OES Yang Liu, Liu Xinqun, Wang Jin (Zhuzhou times new material Polytron Technologies Inc technology center, Hunan, Zhuzhou 412007) Abstract: a method for determination of lead, cadmium and mercury in Zinc Oxide by inductively coupled plasma atomic emission spectrometry (ICP-OES) has been developed. The interference of matrix zinc was eliminated by matrix matching, and the working parameters and conditions were optimized. The detection limits of Pb, Cd and Hg were 0.0474 g/mL, 0.0043 g/mL, 0.0574 g/mL, respectively. The relative standard deviation was between 1.5% and 3.7% (n=5), and the recovery was 94% ~ 106.4%. The method is rapid, accurate and sensitive. It is suitable for the determination of lead, cadmium and mercury in Zinc Oxide. Keywords: ICP-OES; ROHS directive; rubber industry; Zinc Oxide; lead; cadmium; mercury In recent years, due to the introduction of the ROHS directive, environmental protection laws and regulations and regulations and a series of REACH, forming a green barrier of rubber products in Chinas exports, Chinas rubber production industry is facing tremendous pressure on environmental protection [1]. Zinc Oxide is an essential raw material for rubber and tire industry. It is often used as a vulcanizing agent and a reinforcing agent for natural rubber, synthetic rubber and latex. Zinc Oxide often contains heavy metal impurities. The content of lead, cadmium and mercury is directly related to whether rubber products can be detected by ROHS. Therefore, it is of great significance to study the method of rapid determination of heavy metals in Zinc Oxide. The determination of heavy metals in Zinc Oxide mainly consists of chemical and atomic absorption spectrophotometry, [2][3]. The time of chemical method is long and the operation is complicated. Atomic absorption spectrometry can only be measured