化工专业毕业设计—精馏塔的设计.docVIP

河 北 工 业 大 学 毕业设计说明书 作 者： 郭文娟 学 号： 071131 学 院： 化工学院 系(专业)： 化学工程与工艺 题 目： 30000吨苯酐/年装置 产品精制工段（成品塔）的工艺设计 指导者： 赵茜 讲师 评阅者： 2011 年 月 日 毕业设计中文摘要 30000吨苯酐/年装置 产品精制工段（成品塔）的工艺设计 摘要： 本设计选题为3.0×10/年苯酐生产车间的工艺设计。通过各种生产技术路线的评价比较，确定了目前国内外比较先进而又经济合理的以邻二甲苯为原料，采用V2O5为主催化剂的固定床反应器，热熔箱回收产品及连续减压蒸馏得到成品的成熟工艺技术，设计中用模拟法（上机运算）对重点设备成品塔进行了详细计算和结构设计，进行了车间全部设备的计算与设计选型，按施工图的深度和规范认真设计并绘制了车间管道仪表流程图、重点设备反应器的装配图、车间设备布置图、部分工段的管道布置图，对车间用能进行了有效的节能方案与措施，对副产物回收与三废治理提出了经济可行的方案，对车间产品进行经济核算，对项目的经济性和先进性进行了分析研究，提出了具体的车间管理措施及生产操作规程，为项目的顺利建厂投产准备了较为详尽的图纸与资料。 关键词： 邻二甲苯 苯酐 精制 毕业设计外文摘要 Title the Process Design of Refined Section (Finished Tower)of 30,000 t/a Phthalic Anhydride Product Abstract The topic of the design is the phthalic anhydride production process of 3.0 × 104 t/a. Through the evaluation and comparison of diversified production process routes, we have determined the more advanced and economic production technology. The mature process takes O-Xylene as raw material and V2O5-based as catalyst, using a fixed-bed reactor, hot-melt tank which collects the products and continuous vacuum distillation recycling products. In the design the key equipment rectifying tower is calculated and designed in detail with model method (calculated by computer ) ，and all equipments in the plant are calculated and selected, according to construction plans depth and specification, the plant pipe instrument flow sheet, the key equipment’s assembly diagram, the equipment arrangement diagram, and part of piping arrangement diagram are designed and drew carefully .The energy using of the plant is also calculated and analyzed in detail. We also have advanced economic feasible project about the recovery of by-products and the disposal of three kinds of was