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强化氧化对石煤钙化焙烧提钒的影响-中南大学学报
42 1 () Vol.42 No.1
2011 1 Journal of Central South University (Science and Technology) Jan. 2011
( 410083)
950 3 h
6%63%
MnO2 2
0.48 L/h 69% MnO2 ()3%68%
V5+
TF841.3 A 1672−7207(2011)01−0007−04
Effect of oxidation on vanadium extraction from stone coal with
calcified roasting
LI Chang-lin, ZHOU Xiang-yang, WANG Hui, ZHANG Tai-kang, LI Jie, OU Xing, JIANG Xiao-duo
(School of Metallurgical Science and Engineering, Central south university, Changsha 410083, China)
Abstract: The calcified roasting condition for vanadium extraction from stone coal was studied. Under the condition of
950 , roasting 3 h, CaCO3 addition 6% (mass fraction), the subsequent vanadium leaching efficiency of about 63% can
be obtained. On the base of the same condition, effect of air sparging and MnO2 addition on vanadium extraction was
investigated. The reason why oxidation can improve vanadium leaching was investigated through phase and valence state
of vanadium analysis. Results show that vanadium leaching efficiency of 69% can be obtained with air sparging speed of
0.48 L/h and 68% with MnO2 addition of 3%. It is found that oxidation is effective to destroy the ore structure and
increase the percentage of V5+ in calcine, and more calcium vanadate compounds is generated, which easily responds to
acid leaching.
Key words: calcified roasting; vanadium; stone coal; oxidation
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