表面增强拉曼光谱活性基底的制备及其应用研究-食品安全质量检测学报.pdfVIP

5 5 Vol. 5 No. 5 2014 5 Journal of Food Safety and Quality May. , 2014 * 贾宝申, 哈斯乌力吉 , 林 翔, 杨 芳, 林 爽, 吕志伟 ((), 150080) 摘 要: 目的 (surface-enhanced Raman scattering, SERS), 方法 (SEM)- , SERS , , 结果 1 mg/kg , , 1~5 mg/kg , R2=0.928结论 SERS , 关键词: ; ; ; Preparation of Raman surface-enhanced scattering substrate and its application * JIA Bao-Shen, HA-SI Wu-Li-Ji , LIN Xiang, YANG Fang, LIN Shuang, LV Zhi-Wei (National Key Laboratory of Science and Technology on Tunable Laser, Harbin Institute of Technology, Harbin 150080, China) ABSTRACT: Objective Silver colloid was prepared and it was used to detect urotropine in rice noodle. Methods Silver colloid was characterized by scanning electronic microscopy(SEM)and UV-vis absorption spectra. In order to improve the colloid, NaCl was used as aggregating agent. The Raman surface-enhanced scattering (SERS) spectra of urotropine were investigated based on the self-prepared colloid. SERS was used to detect urotropine in rice noodle. Results The limit of qualitative detection was 1 mg/kg. The method showed a good linearity in the range of 1~5 mg/kg for urotropine with R2=0.928. Conclusion This method has the advantages of simple pretreatment, low