水热法合成Pb2Te3O8及其物性研究.pdf

Modern Physics 现代物理, 2017, 7(3), 44-51 Published Online May 2017 in Hans. /journal/mp /10.12677/mp.2017.73007 Physical Properties Studies of Pb Te O 2 3 8 Synthesized by Hydrothermal Method 1 1,2* 1,2 Yan Ma , Wendan Wang , Linji Zhang 1 Key Laboratory of Advanced Technologies of Materials, School of Physical Science and Technology, Southwest Jiaotong University, Chengdu Sichuan 2 Key Laboratory (for Universities) of High Pressure Science and Technology, Southwest Jiaotong University, Chengdu Sichuan th th st Received: May 8 , 2017; accepted: May 28 , 2017; published: May 31 , 2017 Abstract Pb Te O samples were prepared by hydrothermal synthesis. The phase and structural parame- 2 3 8 ters of the synthesized Pb Te O sample were determined by Rietveld refinement of the observed 2 3 8 powder XRD data. The infrared absorption spectra, ambient pressure and high pressure Raman spectra of Pb Te O were measured. The infrared absorption peak of Pb Te O was determined by 2 3 8 2 3 8 infrared spectroscopy. The high-pressure Raman study was carried out at room temperature by using a diamond anvil, and the Raman spectra were measured in the range of 0.3 - 21.8 GPa. By analyzing the frequency shift and splitting of the Raman peak, it is found that the frequency of all the vibrational modes varies monotonically and without the presence of n