【精选】A simple and green procedure for the synthesis of symmetrical.pdf

【精选】A simple and green procedure for the synthesis of symmetrical.pdf

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【精选】A simple and green procedure for the synthesis of symmetrical

Issue in Honor of Prof. (Mrs.) Asima Chatterjee ARKIVOC 2003 (ix) 14-20 A simple and green procedure for the synthesis of symmetrical N,N -disubstituted thioureas on the surface of alumina under microwave irradiation * # Brindaban C. Ranu, Suvendu S. Dey, and Santanu Bag Department of Organic Chemistry, Indian Association for the Cultivation of Science, Jadavpur, Calcutta – 700 032, India E-mail: ocbcr@iacs.res.in # Summer project student from IIT, Kanpur during May-July, 2003 th Dedicated to Professor (Mrs.) Asima Chatterjee on the occasion of her 85 birthday (received 04 Nov 03; accepted 03 Dec 03; published on the web 19 Dec 03) Abstract A variety of symmetrical N,N-disubstituted thioureas have been prepared by a simple reaction of amines and carbon disulfide on the surface of alumina under solvent-free microwave irradiation. Keywords: Thiourea, amine, carbon disulfide, microwave, alumina Introduction The development of simple and eco-friendly synthetic procedures constitutes an important goal in organic synthesis. Many organic solvents, particularly chlorinated hydrocarbons that are used in large quantities in organic reactions are potential threat to human health and environment. Thus, redesign of chemical reactions under solvent-free condition gets a renewed interest. The use of inorganic solid supports such as clay, zeolite, alumina, silica gel for the generation of small organic molecules under solvent-free condition has gained immense popularity beca

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