分离苯—甲苯的工艺设计与换热优化.doc

摘 要 本次设计是分离苯-甲苯的工艺流程设计与换热优化，处理量为10万t/a,苯的纯度大于98.5%，泡点进料。主要任务是精馏塔与换热网络的设计。因苯与甲苯存在着较大的相对挥发度，所以采用连续性精馏对其实现分离。通过基础数据对塔进行设计，包括精馏塔的塔体工艺尺寸的确定、塔板主要工艺尺寸的确定及操作条件的确定，设计结果为塔径为1.8m,塔高为8.6m,进料温度为88.5℃,塔顶温度为81.1℃,塔底温度为107.5℃,塔板数为20层等。塔顶用工业用水对苯进行冷却，通过计算得出冷凝器型号为F-400-Ⅳ-2.5-32。塔底用高温水蒸气对甲苯加热，然后用塔底的甲苯对原料进行预热，之后用加热过甲苯的高温蒸汽对原料加热至泡点温度，再沸器的型号为FB-500-Ⅱ-1.6-42.8,塔底产品加热原料的换热器型号为,高温蒸汽加热原料的换热器型号F500-Ⅳ-2.5-33.2。最终实现节能为3.8×107kJ/h。本次设计还配备了储罐、管道和温度计、流量计、液位计、压力表等附属设备。最后确定出了合适的工艺流程，这将为工业设计提供参考依据。 关键词： 苯,甲苯,换热器,换热网络,精馏塔 Abstract The design is the separation of benzene – toluene and the optimization of heat exchanger.The through-put is 100,000t/a,the purity of benzene is more than 98.5%, the temperature of feed isbubble point temperature.The Main task is design of fractionating-tower and heat exchanger networks.The relative volatility between b-enzene and toluene is enough, so adopt continuous distillation to separate them. Design the tower by the basis of data, including the size of fractionating-tower,the size of plate andDetermination of operating conditions. Planungsergebnis: towerdiameter is 1.8m,the height of tower is 8.6m,the feed tempeture is 88.5℃,the top temputer is 81.1℃,the bottom temputer is 107.5℃ and the plate is 20 etc. Industrial water is used for colling the benzene at the top, the condenser model is F-400-Ⅳ -2.5-32 by Calculating,using vapor with high temperature heating to heat toluene at the bottom. Toluene have been used after the heating of the raw materials of high temperature steam is heated to bubble point temperature, reboiler model is FB-500-Ⅱ -1.6-42.8, the heat exchanger model is which the product of bottom heat the raw materials.The modle of heat exchanger is F500-Ⅳ -2.5-33.2 which High-temperature steam heated the feed. Eventually energy-saving is 3.8×107kJ/h。The design is also equipped with storage tanks, piping and thermometers, flow meters, level gauge, pressure gauges and other ancillary equipments. Finally,determine a suitable process. This will provide