定心藤中酚性成分.pdfVIP

• 838 • ( ) 中华中医药杂志 原中国医药学报 2011年4月第26卷第 4期 CJTCMP , April 2011, Vol . 26, No.4 ·研究报告· 定心藤中酚性成分的研究 1,2 1 曾立 ，尹文清 1 （广西师范大学化学化工学院有机化学教研室药用资源化学与药物分子工程教育部重点实验室，桂林 541004；2湖南省邵阳医学高等专科学校药学系，邵阳 422000） 摘要： 目的：研究定心藤中酚性成分。方法：用色谱技术进行分离，波谱法进行鉴定。结果：从定心藤中 分离得到6个酚性化合物，依次鉴定为青藤碱(Ⅰ)、香草醛(Ⅱ)、白杨素(Ⅲ)、香草酸(Ⅳ)、槲皮素(Ⅴ)、没食子酸 (Ⅵ)。结论：所有化合物均首次从该植物中分离得到。 关键词：定心藤；酚性成分；提取分离 基金资助：药用资源化学与药物分子工程教育部重点实验室科研项目（No.桂科03），广西自然 科学基金创新团队项目（No.2010GXNSFF013001） Study of phenolic compounds from Mappianthus iodoies ZENG Li1,2, YIN Wen-qing1 1 ( Key Laboratory of Ministry of Education of China for the Chemistry and Molecular Engineering of Medicinal Resources, Department of Organic Chemistry, School of Chemistry Chemical Engineering of Guangxi Normal University, Guilin 541004, China; 2Department of Pharmacy Affunan, Shaoyang Medical College, Shaoyang 422000, China ) Abstract: Objective: Study the phenolic compounds from Mappianthus iodoies. Methods: The column of silica gel was employed for the isolation and purifi cation of the phenolic compounds,the structures of the compounds were identifi ed by physiochemical properties and spectral analysis.Results: Six phenolic compounds were isolated from Mappianthus iodoies,Their structures were determined by spectroscopic analysis to be vanillin sinomenine( ), Vanillin( ), chrysin( ), vanillic acid ( ), Ⅰ Ⅱ