【精选】1--Pesticide residues in grapes and during vinification process1--Pesticide residues in grapes and during vinification process.pdfVIP

ARTICLE IN PRESS Food Control xxx (2010) xxx–xxx Contents lists available at ScienceDirect Food Control journal homepage: www.elsevi /locat e/foodcont Pesticide residues in grapes and during vinification process * ˇ ˇ ˇ ˇ Franc Cuš , Helena Baša Cesnik, Špela Velikonja Bolta, Ana Gregorcic Central Laboratories, Agricultural Institute of Slovenia, Hacquetova 17, 1000 Ljubljana, Slovenia a r t i c l e i n f o a b s t r a c t Article history: Pesticide residues in vinification process of two white and two red grapevine varieties were monitored Received 13 January 2010 during the 2007 vintage. Crushed grapes, cake, must, lees and wine were sampled during the vinification Received in revised form 30 March 2010 process. Additionally, grapes were sampled during the ripening process. All samples were taken in trip- Accepted 6 April 2010 licate and analyzed for the presence of 117 pesticides. The pesticide residues were determined by three Available online xxxx validated internal analytical methods: the multi-residual GC-MS method (71 pesticides), the multi- residual LC-MS-MS method (45 pesticides) and GC-MS method for the determination of dithiocarbamates Keywor