苏木色素的提取工艺及染色性能.docx

专题研究苏木色素的提取工艺及染色性能吴慧慧1,侯秀良1,张新龙2,高卫东1,高海燕3(11江南大学生态纺织教育部重点实验室,江苏无锡214122;21江苏省海澜集团,江苏江阴214426;31江南大学化学与材料工程学院,江苏无锡214122)摘要:研究植物染料苏木在提取前的准备,优化苏木提取温度、时间、次数等,测试苏木染液的放置稳定性、酸碱稳定性,及苏木染液质量分数与电导率的关系,并对巴西林、苏木染液染毛织物的方法做了讨论。结果表明:苏木在提取前需将心材粉碎为适当粒度,以保证原料混合均匀;100℃提取,每次提取60min,提取3次;苏木提取液在酸性条件下较稳定,碱性条件下不稳定,变化很大;苏木染液质量分数在0～018%范围内,质量分数与其电导率成正比关系,在水溶液中稳定存在;苏木染料适于采用铝前媒染染色方法染毛织物。关键词:苏木;植物染料;提取工艺;染色性能中图分类号:TS193162文献标识码:A文章编号:100321456(2009)1020001205ExtractionprocessofSappanWoodDyeanditsdyeingpropertiestowoolfabricsWUHui2hui1,HOUXiu2liang1,ZHANGXin2long2,GAOWei2dong1,GAOHai2yan3(11KeyLaboratoryofScienceandTechnologyofEco2Textile,MinistryofEducation,JiangnanUniversity,Wuxi214122,China;21HeilanGroup,Jiangyin214426,China;31SchoolofChemicalandMaterialEngineering,JiangnanUniversity,Wuxi214122,China)Abstract:Inthisarticle,theextractionprocessesofSappanWoodDye(SWD)anditsdyeingpropertiesareinvestigated.Theextractionprocessesincludethepreparationbeforetheextractionwithwater,andthetemperature,periodandsoonduringtheextractionwithwater.Thedyeingpropertiesincludeitsstabilityduringtheplacementanditsstabilitytoacid,alkalineanditsconductivityofthedyeliquidwiththedifferentcontent.ThedyeingmethodofSWDandBrazilin(oneofthemainchemicalofSWD)isalsodiscussed.ItshowsthatSappanWoodshouldbecrushedtotheappropriateparticlesizetoensuretheuniformmixingofrawmaterialsbeforetheextraction;Extractionprocesses:100℃,60mineverytimeand3times;SWDliquidismorestableunderacidicconditions,anditisinstableunderalkalineconditionsanditchangesgreatly;Intheliquidcontentof0～018%,itselectricalconductivityisdirectlyproportionaltotheconcentrationofSWDandthecolorationmolecularofSWDcanexistsstablyinwater;Pre2mordantdyeingmethodwithmordantaluminumissuitablefordyeingwoolfabricswithSWD;BesidesthemajorcomponentsBrazilincandyewoolfabric,theothercomponentsinSWDcanalsodyewoolfabric.Keywords:SappanWood;vegetabledye;extractionprocess;dyeingproperties收稿日期:2009-03-10基金项目:江南大学创新团队发展计划,江苏省博士后科研资助计划项目(项目编号:0602006B)作者简介:吴慧慧,硕士,主要从事天然染料的纯化及其在纺织中的应用。通讯作者: