双炉双塔分离生产工业萘的工艺设计.doc

目 录 摘 要 1 ABSTRACT 2 1文献综述 3 1.1 焦化工业发展史 3 1.1.1焦化工业的地位 3 1.1.2国外焦化生产现状 4 1.1.3国内焦化生产现状及问题 5 1.1.4中国焦化工业的发展方向 7 1.2煤焦油加工 8 1.2.1 中国煤焦油加工企业的分布与工艺特点 9 1.2.2世界煤焦油加工企业的概况与工艺特点 10 1.2.3国内外煤焦油加工工艺的比较 10 1.2.4焦油的连续蒸馏 12 1.3工业萘生产工艺 14 1.3.1工业萘的生产工艺 15 1.3.2双炉双塔连续精馏 16 1.3.3单炉单塔连续精馏 17 1.3.4 单炉双塔加压连续精馏 17 1.3.5提高萘产率和质量的措施 18 1.4本设计拟采用的方案 18 1.5非工艺条件的选择 18 2 设计内容 20 2.1工艺流程的选择 20 2.2初馏塔工艺计算 21 2.2.1初馏塔物料衡算 21 2.2.2 初馏塔的工艺计算 22 2.2.3 初馏塔工艺负荷计算 27 2.2.4 初馏塔尺寸的计算 30 2.2.5 初馏塔塔板主要工艺尺寸的计算 33 2.2.6 初馏塔塔板流体力学的验算 35 2.3 精馏塔工艺计算 45 2.3.1精馏塔物料衡算 45 2.3.2 精馏塔的工艺计算 48 2.3.3精馏塔工艺负荷的计算 52 2.3.4精馏塔尺寸的计算 55 2.3.5 精馏塔塔板主要工艺尺寸的计算 57 2.3.6 精馏塔塔板流体力学的验算 60 2.4 机械校核 68 2.4.1 精馏塔的机械校核 68 2.5 热量衡算 81 2.5.1 初馏塔酚油冷凝冷却器 81 2.5.2 工业萘冷凝器 82 2.6 管式炉的设计 83 2.6.1初馏塔管式炉 83 2.6.2 精馏塔管式炉 85 2.7非工艺条件 86 2.7.1土建设计条件 86 2.7.2采暖通风设计条件 87 2.7.3 电器与动力设计条件 87 2.7.4 给排水设计条件： 88 2.7.5 分析化验条件 89 3 结论 90 参考文献 92 致 谢 93 摘 要 该设计采用的是酚、萘、洗通过双炉双塔分离生产萘的工艺设计关键设备选型的原则和结构参数,及工艺作了简要阐述ABSTRACT This article introduces the process design of rectification separation of naphthalene from wash oil with twin furnaces and twin column. It also recounts several considerations and comprehensive parameters of selecting the key separation unit as well as the production results and the process optimization. The process of design and calculation process are: raw material for producting naphthalene is the multi-component mixture fraction. Theoretical plate numbers are achieved by their multi-component mixtures distillation to the calculation of the law. System in the twin towers, two tower no lateral line product, it may be the key component method to calculate. First material balance, obtain the composition of raw materials. Tower operating conditions must determine the operating pressure and the top, bottom temperature. operating pressure used to near atmospheric pressure. The top temperature of the tower is determined by the composition of distillates and the total pressure of the top of the tower. Bottom temperature is determined by