多晶X射线衍射仪试验技术基础-分析测试中心.PDF

多晶X射线衍射仪试验技术基础-分析测试中心.PDF

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多晶X射线衍射仪试验技术基础-分析测试中心

X 微构分析实验室 多晶 射线衍射仪实验技术手册 多晶X 射线衍射仪 实验技术基础 布 莱 格 科 技 ( 北 京 ) 有 限 责 任 公 司 I · · X 微构分析实验室 多晶 射线衍射仪实验技术手册 目    录 前 言·································································································· 1 第一章 X射线基础·················································································· 3 1.1 概述····························································································· 3 1.2 X 射线的产生················································································· 5 1.3 X 射线管工作条件的确定·································································· 6 1.4 X 射线光谱···················································································· 8 1.4.1 连续光谱·············································································· 8 1.4.2 特征光谱·············································································· 9 1.5 物质对X 射线的吸收,实验波长及滤波片的选择··································11 1.5.1 线吸收系数··········································································11 1.5.2 质量吸收系数·······································································11 1.5.3 吸收系数与波长及元素的关系················································· 12 1.5.4 实验波长的选择··································································· 12 1.5.5 滤波片················································································13 1.6 晶体对X 射线的衍射······································································ 13 1.6.1 衍射方向·····························

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