马蹄螺珍珠层粉微量化学成分分析.PDFVIP

※分析检测 食品科学 2010, Vol. 31, No. 22 349 1 1 1 2 2 刘石生 ，李斐然 ，王慧敏 ，冯永勤 ，谢珍玉 (1.海南大学食品学院，海南 海口 570228 ；2.海南大学海洋学院，海南 海口 570228) 　 为充分利用去肉后的马蹄螺贝壳资源，从塔形马蹄螺制得珍珠层粉，测定其微量有机物(二氯甲烷萃取) 、 酸不溶性蛋白质氨基酸组成及微量无机元素。结果表明：在二氯甲烷萃取物中共检测出 13 种成分，质谱数据库确 定 9 种成分。从酸不溶蛋白质中检出 18 种氨基酸，含有人体所需的 8 种必需氨基酸；微量元素定量检测结果表明， 马蹄螺珍珠层粉中含有人体所需的 Mg 、Fe 、Zn 、Se 等微量无机元素，同时含有微量的 As 、Hg 、Pb ；半定量 检测检出 27 种微量元素。因此，马蹄螺珍珠层粉是一种值得开发的资源。 马蹄螺；珍珠层粉；酸不溶蛋白质；微量元素 Organic Components, Amino Acids and Inorganic Elements in Pearl Nacre Powder of Trochus pyramis Born 1 1 1 2 2 LIU Shi-sheng ，LI Fei-ran ，WANG Hui-min ，FENG Yong-qin ，XIE Zhen-yu (1. College of Food Science and Technology, Hainan University, Haikou 570228, China； 2. College of Ocean, Hainan University, Haikou 570228, China) Abstract ：Organic components in methylene dichloride fraction, amino acid in acid-insoluble fraction, and minerals in and inorganic elements in pearl nacre powder prepared from Trochus pyramis Born were investigated. GC-MS analysis showed the existence of 13 compounds in methylene dichloride fraction, and 9 compounds were identified. Totally 18 kinds amino acids, including 8 kinds essential amino acids, were found in the acid insoluble fractions by automatic amino acid analyzer. Inorganic elements, such as Mg, Fe, Zn, Se, as well as As, Hg, Pb were found and determined by using inductively coupled plasma mass spectrometry. The shell of Trochus pyramis Born is a resource worthy of development. Key words ：Trochus pyramis Born ；pearl nacre powder ；HCl-insoluble protein ；trace chemical 中图分类号：R284.1　　　 文献标识码：A 文章编号：1002-66