LZ91双相型镁锂合金显微组织与拉伸性质之热处理效应研究.pdf

LZ91雙相型鎂鋰合金顯微組織與拉伸性質之熱處理效應研究 楊崇煒, 陶亮熒, 陳至豪 國立虎尾科技大學 材料科學與工程系 摘 要 本研究採用LZ91鎂-鋰-鋅合金擠型材，探討 (α/β)雙相LZ91-F施以不同退火熱處理後之微 觀組織解析，以及在不同變形溫度、改變應變速率下之拉伸機械性質變化。相組成百分率和 XRD分析結果發現LZ91經熱處理後β相所占比例會提升，而且當熱處理溫度在200ºC 以上時晶 粒徑會增大，同時α相會有明顯的圓鈍化趨勢 ，硬度值隨著持溫時間越久及β相的增加而逐漸 下降。在室溫、100ºC 、150ºC變形溫度進行拉伸試驗，LZ91-F之降伏強度(YS) 、抗拉強度(UTS) 與均勻延伸率(UE)皆隨拉伸溫度升高而降低，而總延伸率 (TE)則隨拉伸溫度升高而提升達約 −3 − 1 −3 − 1 −4 − 1 55% ；不同初始應變速率(3.34 × 10 s , 1.67 ×10 s 及8.35 ×10 s )之結果發現LZ91-F之YS 與UTS隨應變速率增加而提高， TE則隨應變速率增加而降低，以較慢應變速率拉伸具有較佳 延伸率。LZ91-F 以200ºC 與300ºC進行退火處理發現α相在高溫與長時間熱處理會有固溶效 應，α相呈等軸晶且所佔面積率減少，熱處理後之LZ91合金之晶面方位與拉伸性質差異不大。 關鍵詞：鎂 -鋰合金，雙相鎂合金，拉伸機械性質，應變速率 Abstract The dual-phase Mg-Li-Zn extruded alloy (LZ91-F) was used in this study. The main subject of present study is to evaluate microstructural evolution for the α/β-dual phase LZ91-F with various annealing heat treatments. Tensile mechanical properties of LZ91-F at different deformation −3 − 1 −3 − 1 −4 temperatures (RT, 100ºC, 150ºC) and initial strain rates (3.34 × 10 s , 1.67 ×10 s 及8.35 ×10 s− 1) were also studied. Experimental results indicated that the volume fraction of β-phase and the grain size are increased after heat treatment, especially higher than 200ºC. The microhardness of LZ91 alloy is decreased with increasing heat treating time and the β-phase content. YS, UTS and UE were decreased, whereas TE was increased to about 55% with increasing deformation temperatures for LZ91-F. The YS and UTS of LZ91-F were increased, whereas the TE was decreased with increasing initial strain rates. The LZ91-F showed better elongation with performing lower initial st