介孔纳米TiO2的超声化学法合成及其表征.pdfVIP

24 2 Vol. 24, No. 2 2005 3 ENV IRONMENTAL CHEM ISTRY M arch 2005 TiO * 2 包 南 马 东 尚贞晓 孙 剑 张 锋 刘廷礼 (, , 250100) T iO , XRD, TEM, FTIR , 2 , TiO ; , 2 T iO , T iO , 2 2 , , , ( IUPAC) , 2 50nm [ 1] , , , , . , [ 2, 3] . [ 4, 5] , , [ 6, 7 ] , T iO , XRD, TEM, FTIR 2 1 11 T iO 2 40m l 10m l A ; 00033mol 001mol 10m l B ( Son ics and M aterials, VCX 500, 20kH z, 100W cm- 2 ) 13mm A , B, 80, 450 2h, TC 12 12 R igaku D /MAXAX ( XRD, CuK , 40kV ) ; JEOL JEM100CX (TEM ) ; N icolet20SX ( FTIR) , KBr 2 21 XRD 1TC XRD 1, 2 2532, 5492 6264, 12 ( 101)( 211) ( 204) , 450 2h, , , ( 2004 9 15) . 863 ( 2003AA601060- 01- 04), ( 11440053187025) . , Em ail: baonan@ sdueducn 2 : T iO 151 2 T iO T iO , Debye 2 2 ScherrerT iO 30nm 2 1 TC XRD 12 F ig1 XRD pattern of the sam ple TC12 22 TEM 2 450 2h TC TEM . 2, , 12 20 100nm, , . 3