NAA using Kayzero from peak area to element concentrationsNAA使用KAYZERO元素浓度的峰面积.pptVIP

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2018-04-17 发布于江西
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NAA using Kayzero from peak area to element concentrationsNAA使用KAYZERO元素浓度的峰面积.ppt

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NAA using Kayzero from peak area to element concentrationsNAA使用KAYZERO元素浓度的峰面积.ppt

NAA using Kayzero:from peak areas to element concentration R. van Sluijs, k0-ware, Heerlen, the Netherlands D. Bossus, DSM Geleen, the Netherlands F. De Corte, RUG, Ghent, Belgium Problem? No problem!? No problem,but ..... (1) How to get the correct peak area? Use a perfect gamma spectrometry system and keep it in the best possible condition! Use the perfect gamma spectrum deconvolution program! However: who has this perfect set-up? No problem, but......... (2) How to select the analytical line K0-library has data for 68 elements, 144 nuclides and more than 700 gamma-lines For a panoramic analysis you use preferably 2 irradiations (short and long) each followed by 2-3 measurements A single element will give data for several nuclides and probably tens of gamma lines. All we want one single list: Containing the all elements with their concentrations and/or limits of detection. DSM’s/Kayzero’s method Optimise the peak table! Peak Table: Area’s and Energies from gamma spectrum deconvolution program Calculation Concentrations for all lines in the k0- library Evaluation Identify the nuclides in the sample Correct for gamma interferences Calculate averages per nuclide and per element Average over all measurements Refine the results Optimise the peak table! Peak Areas: Broadened peaks (due to count rate effects, bad pile-up correction, etc..) can be split by the gammaspectrum deconvolution program into two separate peaks. Sum the false/artificial peaks for a correct result Peak locations: Linear energy calibration, non-linear is often better Re-do the energy calibration Hypermet shifts data 1 channel to the left Shift back Measurement Input screen Peak summation screen Re-do energy calibration k0-calculations Calculate concentrations for all library lines Including Corrections for: background, dead-time, gamma-absorption, burn-up, neutron self absorption, True-coincidence correction No matching peak: the LD concentration is calculated using