YF3纳米材料合成水热合成不同形态YF3纳米线及其表征推荐.docVIP

水热合成不同形态YF3纳米线及其表征 摘 要 本课题采用以NH4F为氟源，Y(NO3)3为钇源，在不同反应温度，不同PH值的条件下，通过简单的水热法合成了纳米粉体沉淀，经洗涤、过滤、干燥粉碎、真空脱水制得不同形态的氟化钇晶体，再经过X射线衍射(XRD)结果表明所得的产物确实为YF3晶体。用扫描电子显微镜(SEM)和透射电子显微镜(TEM)对产物的形貌表征，表明产物是纳米线结构 关键词：纳米线，水热合成，YF3 Room temperature, controlled synthesis of nanowires of different forms and Characterization YF3 ABSTRACT This topic used to NH4F as the fluoride source, Y (NO3) 3 as the yttrium source, at different reaction temperatures, under conditions of different PH values, by a simple hydrothermal synthesis of nano powder precipitation, washing, filtration, dried and crushed vacuum dehydra