纳米氧化锌的制备、表征及其光学性质分析-材料物理与化学专业论文.docx

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纳米氧化锌的制备、表征及其光学性质分析-材料物理与化学专业论文.docx

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纳米氧化锌的制备、表征及其光学性质分析-材料物理与化学专业论文

StudyoFFabrication ,CharacterizationandOpticalPropertiesofZinc Oxide Nanostructure(Zhang Jian-weiMaterials Physics and Chemistry)Abstract：Asawide-bandgapsemiconductormaterialwith3.37eVbandgapenergy and60meVexcitonbondageenergy,thewurtzitestructuralzincoxide(ZnO)isideal materialappliedtofabricateultravioletphotoelectrondevice.Duetosmallsizeeffect andquantumconfinementeffect,nanostructuralZnOislargelysuperiortoitsbulk materialinthephysicspropertiesandpromisingtobeusedtoconstructmicro/nano ultravioletlaser,ultravioletemissiondiodeandhigh-sensitivebiology/chemistry sensor.TheindustrializationofnanostrualZnOis thefabricationofthenanomaterials. AlthoughsomeZnOnanostructureswithdifferentmorphologieshavebeenfabricated byvariousmethodsbynow,thefactorsinfluencingcrystalgrowthprocesscan’t efficientlycontrolled,andtheobtainednanostructuresstillexistlargeuncertaintyin morphologyandphysicsproperties.Inparticular,theunderstandingonthegrowth mechanismstillkeepsalowerlevel.Therefore,thefabricationofZnOnanostructures willstillbeanimportantpartofZnOresearchworkinalongtime.Thispaperreviews thenatureofZnO,fabricationmethods,testingmethods.SomeZnOnanostructures were successfully synthesized by chemical vapor deposition(CVD) and thermalevaporation techniques. The morphologies，crystalline qualities and opticalcharacteristicsofZnOnanostructureswereinvestigatedbyscanningelectron microscopy(SEM)，X-raydiffraction(XRD),EnergyDispersiveX-raySpectrometry(EDS)andPhotoluminescence(PL)analytictechnology,respectively.Thedetailsare asfollows:Inthispaper,asimplemethodforfabricatingZnOnano-disksisgiven,andZnO nano-disks with sizeaboutseveralmicronsandthicknessabout400nmobtainedonSi substrates(100)intheatmosphere,withZnpowerthermallyevaporateddirectlyin thecrucible.X-raydiffraction(XRD)revealsthegrownsamplesarehexagonalZnO crystal.Scanningelectronmicroscopy(SEM)imagesshowthatthemorphologyand sizeofsamplesis closelyrelatedtotheevaporationtemperatureofzinc.Thephotoluminescence(PL)spectrumatroomtemper