al2o3陶瓷的自身晶须连接及其与tc4钛合金的钎焊分析word格式论文.docx

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al2o3陶瓷的自身晶须连接及其与tc4钛合金的钎焊分析word格式论文.docx

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al2o3陶瓷的自身晶须连接及其与tc4钛合金的钎焊分析word格式论文

AbstractAluminaisakindofmaterialwidelyusedinspaceindustry,chemicalindustry,etc. duetoitslowelectricalconductibility,excellentmechanicalstrengthandhighthermal insulationcapability.Residualstresstendstobeproducedinthejointofceramictometal duetothemismatchofthepropertiesbetweenthem.Thejoiningofceramics with ceramicormetalwasrealizedwiththehelpofwhiskers.Whenjoiningceramicswith ceramics,whiskersweresynthesizedbothonthesurfaceoftheceramicsandintheseam toformthejoint.Whenjoiningceramicwithmetal,whiskerswerefirstlygrownonthe surfaceoftheceramicsandthenbrazedwithmetal.Themorphologyofthewhiskersand themicrostructurerevolutionaswellasthevariationofthestrengthofthejointswere researched bymeans of SEM, EDS, XRD and strength test.Al18B4O33andAl4B2O9whiskersweregeneratedonthesurfaceofaluminaceramics with B2O3and Al2O3as raw materialsand K2SO4,Fe2O3, MnO2as flux. Thelength of the whiskersrangesfrom5-20μm,andthediametersofthewhiskerswereabout1-2μm.The growthdirectionofmostwhiskershadasmallangletothesurfaceoftheceramics.With theincreaseoftheholdingtimeandthetemperature,thelengthofthewhiskersfirstly grewandthenremainedthesame.WhenK2SO4wasusedasflux,thelengthofwhiskers grewupto15-20μm.WhenMnO2wasusedasflux,thegrowthdirectionofmost whiskers had alargeangleto thesurfaceof the ceramicsAluminawasjoinedtoitselfinairenvironmentbyB2O3+Al2O3powdermixtureas theinterlayertosynthesizealuminumboratewhiskersinthejoint.Themicrostructure evolutionwasanalyzedbymeansofscanningelectronmicroscope(SEM)andX-ray diffraction(XRD).Thepossiblemechanismofmicrostructurerevolutionwasalso discussed.Theeffects ofparameterssuchas heatingcyclesandtemperatureonthe microstructureaswellasthe3-pointflexuralstrengthofthejointwereinvestigated.It wasfoundthatheatingthespecimenforseveralheatingcyclesinsteadofholdingata constanttemperatureforalongtimecaneliminatethevoidsamongthewhiskersto achieveadensemicrostructure,andthephenomenonthathighertemperaturescan acceleratethereactionwasalsoobserved.Thehigheststrengthofthe jointre