基于慢正电子束流技术制备sio,2薄膜的应用-application of sio _ 2 thin films prepared by slow positron beam current technology.docxVIP

Electro-assisted Self-assembly is a viable method of preparation of SiO2 thin films, This study focuses on the structure of prepared the SiO2 films by different methods and the method of preparation of thin films were discussed. The synthesis and characterization of mesoporous SiO2 film were introduced in this thesis. The microstructure and performances of ordered mesoporous SiO2 film fabricated by sol-gel method were investigated, and the film formation mechanism was discussed. According to the reported Electro-assisted Self-assembly method, we successfully prepared a series of mesoporous SiO2 film. With changing of the reactant ratio, film preparing method, deposit times of sol and film, annealing condition, the influences of the template quality, pH value, deposit times of the sol and film, annealing temperature and heat preservation time on porous structure and film qualities of SiO2 film were studied. The pore structure and the crystalline category of SiO2 film were identified with SEM, XRD, and positron annihilation technique.Positron spectroscopy applicationsisextremelyimportantinmaterialsscience,it has become an important the nuclear analysis methods of material micro structure. based on the our laboratory spectroscopy devices and positron spectroscopy techniques, using of high energy physics designe and build of 22Na slow positron beam equipment to carried out involving the wider field of applied research and slow positron beam devices debugging and measurement.Keywords: SiO2 filmElectro-assisted Self-assemblyMagnetron sputtering Sol- gelslow positron beam独创性声明本人声明所呈交的学位论文是本人在导师指导下进行的研究工作及取得的 研究成果。据我所知，除了文中特别加以标注和致谢的地方外，论文中不包含其 他人已经发表或撰写过的研究成果，也不包含为获得 成都理工大学 或其他教 育机构的学位或证书而使用过的材料。与我一同工作的人员对本研究所做的任何 贡献均已在论文中作了明确的说明并表示谢意。学位论文作者签名：年月日学位论文版权使用授权书本学位论文作者完全了解成都理工大学 有关保留、使用学位论文的规定， 有权保留并向国家有关部门或机构送交论文的复印件和磁盘，允许论文被查阅和借阅。本人授权 成都理工大学可以将学位论文的全部或部分内容编入有关数 据库进行检索，可以采用影印、缩印或扫描等复制手段保存、汇编学位论文。（保密的学位论文在解密后适用本授权书）学位论文作者签名：学位论文作者导师签名：年月日第 1 章引言1.1 选择电辅助自组装制备二氧化硅的意义材料、能源和信息