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化学实验中经常容易犯的安全错误(Safety mistakes often made in chemical experiments).doc
化学实验中经常容易犯的安全错误(Safety mistakes often made in chemical experiments)
Common mistakes in chemical experiments
--------------------------------------------------------------------------------
Author: emking included date: 2006-01-11 release date: 2006-01-11
There are too many experiments in chemistry, and there are too many operations. If you havent done it, you will make mistakes. Learn from these mistakes
The lesson is precious.
So I invite you to talk about the mistakes youve made in your experiments, or the mistakes youve seen in others
Let others learn these precious lessons and not repeat their mistakes.
Im going to start.
React in acid or alkaline conditions, and, if possible, neutralize the product as soon as possible. otherwise
The product may decompose after a long time.
When we run out of heavy methane, we tend to add acid to the rest of the heavy nitrogen methane. A man is bold enough to use it directly
Hydrochloric acid (should dilute hydrochloric acid or acetic acid), and the residual alkali exothermic, ether solution of diazomethane ~ ~ ~ ~ ah
In this way, he conquered the explosion, there is a teacher that is divided into liquid funnel plug not coated with vacuum grease, a friction will be put
The ether is burning. Its horrible
You must pay attention to the use of heavy nitrogen methane, the first time it is better to have experienced people in the guidance, do not yourself
Do, is not too big, NMU at most 25 kebie too much, if you need a large amount of it in several batches to do
Be sure to pay attention to ether in summer. In August this year, I extracted with ether in a separatory funnel, only in the shake up to
Ready to bleed, blow up, but it didnt hurt me. I have a product!!!
One time I made a liquid-liquid extraction, first washed with 50ml HCl organic phase (containing products), and then washed with 50ml 5% NaHCO3
Polyester products, results when shaking the plug is opened, all products are jetted out. The reason is that there is no bleeding.
Yo
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