真空烧结铁基耐磨涂层的制备工艺.docVIP

真空烧结铁基耐磨涂层的制备工艺及组织 摘要:本文采用真空烧结法制备铁基耐磨涂层，其工艺大致为：在45钢基体上涂覆铁基自熔性合金粉，并添加一定比例的硬质相颗粒WC，然后在真空烧结，得到硬质涂层。并且分析了所制备的涂层组织、性能及与基体间的界面结合状况。结果表明：涂层与基体之间具有良好的结合特性。观察维氏硬度以及金相组织X-射线能谱分析以及扫描电镜（SEM）分析了一种新型真空熔结铁基合金涂层的组织结构。铁基合金涂层是以高铬铸铁为粘结相、以大颗粒WC相为硬质相的材料；WC相的体积分数约70%，粘结相是以奥氏体为基体、其中分布有针状相、针状相和粒状相。 关键字: 真空烧结；铁基合金涂层；组织结构 Vacuum sintering iron-based wear-resistant coating of the preparation and organization Abstract: In this study,the high performance wear-resisting coating with Fe-based alloy prepared by the method of vacuum sintering were researched.After painted on the were sintered of 45 steel,the alloy powders that mixed with the hard phase,such as WC,were sintered in the vacuum,and a ood property ard coating was obtained.The microstructure, hardness and the interface between the coating andsubstrate were researched thoroughly. The resuits show that the coating combines on the substrate very well.Observe Vickers hardness and metallographic organization chart, and through the two aluminum alloy X-ray energy spectrum analysis and scanning electron microscopy (SEM) analysis. The microstructure of a new vacuum melting Fe-base alloy coating has been studied.The Fe-base alloy coating is a metal-matrix composite which is composed of high chromium cast iron matrix phase and big particle phase WC of about 70% WC volume fraction.The matrix phase is a solid solution in which phase and phase distribute evenly. Keywords: Vacuum meiting;Fe-base alloy coating ;microstructure 目录 摘要: I Abstract II 1 绪论 1 1.1 选题和研究课题的意义 1 1.2 国内外研究现状和发展趋势 2 1.3 真空烧结基本原理 3 1.3.1 界面元素互扩散与冶金结合的形成 3 1.3.2 浸润性与界面元素互扩散的关系 3 1.3.3 浸润性与熔结涂层连续性的关系 4 1.4 真空熔结的适用范围与应用 4 1.4.1 真空熔结工艺的应用功能 4 1.4.2 真空熔结涂层的适用范围 5 1.5 本文主要研究内容 6 2 实验材料的选择与处理工艺研究 7 2.1 真空熔结涂层的材料和性质 7 2.1.1 元素金属粉 7 2.1.2 合金粉 7 2.1.3 表面硬化合金 8 2.2 真空熔结工艺 8 2.3 各种烧结方法 9 2.4 真空烧结涂层工艺特性 9 2.5 熔结工艺对基体强度的热影响 10 3 实验设备材料和研究方法 11 3.1 实验设备 11 3.2 实验材料 11 3.3 组织分析方法 12 3.3.1 X射线衍射分析 12 3.3.2 扫描电镜分析 12 3.4 实验结果讨论 12 3.4.1 碳化钨涂层的显微组织 12 3.4.2 X-射线能谱分析 20 3.4.3 SEM分析 23 3.4.4 铁基耐磨涂层的硬