熔铸法制备ticti-6al-4v复合材料组织与力学性能研究-microstructure and mechanical properties of tic ti - 6al - 4v composite prepared by fusion casting.docx

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2018-07-29 发布于上海
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熔铸法制备ticti-6al-4v复合材料组织与力学性能研究-microstructure and mechanical properties of tic ti - 6al - 4v composite prepared by fusion casting.docx

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熔铸法制备ticti-6al-4v复合材料组织与力学性能研究-microstructure and mechanical properties of tic ti - 6al - 4v composite prepared by fusion casting

AbstractTiC/Ti-6Al-4Vcompositeswerepreparedbymelting-castingprocessinthisstudy.TiC/Ti-6Al-4Vcompositesarereinforcedwith5%,10%and15%volumefractionofTiCrespectively.ThemorphologyformationandgrowthmechanismsofTiCinthecompositeswereinvestigated.ThecontrolandimprovingmethodsforTiCmorphologywerestudiedanddiscussed.Theeffectofheattreatmentonmicrostructureandpropertiesofthecompositeswasanalyzed.ThetensilepropertiesatbothroomandelevatedtemperaturewereinvestigatedontheTiC/Ti-6Al-4Vcompositesfabricatedbyinductionmelting,andthenthestrengtheningandfracturemechanismsofTiC/Ti-6Al-4Vcompositeswerestudied.ThermodynamicanalysesandXRDresultsshowedthatTiCphaseisstableinmeltedTiC/Ti-6Al-4Vcomposites.ThesolidifiedTiCismainlyeutecticTiCinthecompositeswhenthefractionofTiCissmall,whiletheproportionofprimarydendriticTiCincreasesobviouslywiththefractionofTiCincreasing.ThecompositionforTiCshowedthatthesolidifiedTiCisofcarbondeficiency,ofwhichtheatomicratioofC/Tiiscloseto0.5.ThisleadstoadecreaseforthedensityofsolidifiedTiC.TheresearchonthegrowthmorphologyofTiCindicatedthatthesolid-liquidinterfaceofTiConsolidificationisakindoftransitioninterfaceinmelting-castingTiC/Ti-6Al-4Vcomposites.Thus,thesolidifiedTiCpresentsbothfacetedandnon-facetedgrowthmorphologies.ThereareTiCcrystalnucleuseswithlargesizeinthemelt,whichcouldpromotethetwo-dimensionalnucleationgrowthbydepositingonthesolid-liquidinterfaceofTiConsolidification.Therefore,someTiCdendritesexhibitthelayergrowthmorphologyduetothetwo-dimensionalnucleationgrowthofTiC.TiCpowder,graphitepowderandcarbonblackpowderwithdifferentsizeandstatuswereusedastheCsourcesofTiCintheTiC/Ti-6Al-4Vcomposites.ThestudiesoftheeffectofCsourcesonTiCmorphologyshowedthattheTiCcrystalnucleusissmallerandmoredispersedinthemeltwhenfinecarbonblackpowderwasusedastheCsource.Moreover,thesizeofsolidifiedTiCiscomparativelysmallerandtheprimaryTiCisnoteasytogrowthtodevelopeddendritewiththeCsourceofcarbonblack.Themelting-castingTiC/Ti-6Al-4Vcompositeswereheattreatedatdifferenttemperatur