（毕业论文毕业设计）-PVC-PI复合材料的研究.docVIP

l l PVC/PI复合材料的研究 摘要 此方法是利用聚酰亚胺优异的耐高温、耐绝缘、强的机械力学性能等，利用其聚酰亚胺极性基团和聚氯乙烯极性基团间的相容性，通过共混改性方法，改性聚氯乙烯；使用两步法制备出不同分子量的PI粉末, 测试加入不同分子量和添加量的聚酰亚胺粉末后的复合材料的性能，通过热重分析、力学实验、红外光谱分析、氧指数测定及偏光显微镜分析，选择出热稳定性提高、力学性能优异、阻燃性能好，从而分析探讨不同分子量的PI和不同添加量的PI对复合材料性能的影响。 关键词：聚氯乙烯，聚酰亚胺，分子量，添加量、复合材料  PVC/PI composite materials Abstract This method is the use of polyimide excellent high temperature resistance, insulation, strong mechanical properties, Compatibility between the polar groups of the polyimide and PVC polar groups by the modified method of blending the modified PVC; Two-step method to prepare different molecular weight of PI powder test by adding different molecular weight and the amount of polyimide powder composites, By thermal gravimetric analysis, mechanical tests, infrared spectroscopy, oxygen index and polarized light microscopy analysis, select the thermal stability, excellent mechanical properties, flame retardancy, which analysis to explore the different molecular weight PI and add the amount of PIimpact on the performance of the composite. Keywords: polyvinyl chloride, polyimide, molecular weight, amount of composite materials l 目录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc327196316 1 前 言 PAGEREF _Toc327196316 \h 3 HYPERLINK \l _Toc327196317 1.1 复合材料的研究背景 PAGEREF _Toc327196317 \h 3 HYPERLINK \l _Toc327196318 1.2 研究目的及重要意义 PAGEREF _Toc327196318 \h 5 HYPERLINK \l _Toc327196319 1.3 论文研究内容 PAGEREF _Toc327196319 \h 5 HYPERLINK \l _Toc327196320 2 实验部分 PAGEREF _Toc327196320 \h 6 HYPERLINK \l _Toc327196321 2.1 实验原料及配方 PAGEREF _Toc327196321 \h 6 HYPERLINK \l _Toc327196322 2.1.1 原材料 PAGEREF _Toc327196322 \h 6 HYPERLINK \l _Toc327196323 2.1.2 聚酰胺酸的合成原理 PAGEREF _Toc327196323 \h 6 HYPERLINK \l _Toc327196324 2.1.3 复合材料的配方 PAGEREF _Toc327196324 \h 9 HYPERLINK \l _Toc327196327 2.2 实验仪器 PAGEREF _Toc327196327 \h 10 HYPERLINK \l _Toc327196328 2.3 实验工艺流程 PAGEREF _Toc327196328 \h 11 HYPERLINK \l _Toc327196329 2.3.1 聚酰亚胺的制备 PAGEREF _Toc327196329 \h 11 HYPERLINK \l _Toc3271963