中的多溴二苯醚-食品安全质量检测学报.PDF

7 1 Vol. 7 No. 1 2016 1 Journal of Food Safety and Quality Jan. , 2016 1* 2 1 1 1 李锦花 , 李赛花 , 许海峰 , 陈丹超 , 马 明 (1. , 315012; 2. , 315040) 摘 要: 目的 方法 () 1 cm×1 cm , , -(1:1, V:V), 150 ℃, 1500 psi, 10 min, 3 , -, , 226 nm 结果 8 PBDEs 95%~105%, (n=6)RSD3%, 0.1~0.2 μg/mL, 0.999结论 GB/Z 21276-2007 , ()PBDEs 关键词: ; ; (); Determination of polybrominated diphenyl ethers in corrugated box (cardboard) by accelerated solvent extraction-high performance liquid chromatography 1* 2 1 1 1 LI Jin-Hua , LI Sai-Hua , XU Hai-Feng , CHEN Dan-Chao , MA Ming (1. Technology Center of Ningbo Entry-Exit Inspection and Quarantine Bureau, Ningbo 315012, China; 2. Societe Generale de Surveillance S.A.-China Standard Technology Development Corp. Standards Technical Services Co., Ltd. Ningbo Branch, Ningbo 315040, China) ABSTRACT: Objective To establish a method for the determination of polybrominated diphenyl ethers (PBDEs) in corrugated box (cardboard) by high performance liquid chromatography (HPLC) with accelerated solvent extraction. Methods The corrugated box (card