GB/T 16631-1996柱液相色谱分析法通则.pdf

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2019-01-03 发布于四川
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已被新标准代替，建议下载标准 GB/T 16631-2008
| 1996-12-02 颁布
| 1997-05-01 实施

GB/T 16631-1996柱液相色谱分析法通则.pdf

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ICS71.040.40 c 04 E 中华人民共和国国家标准 GB/T16631一1996 柱液相色谱分析法通则 Generalrulesforanalyticalmethods ofliquidcolumnchromatography 1996一12一02发布 1997一05一01实施国家技术监督局发布 GB/T 16631一 1996 目次一前言苦、工范围 ······，，·········，·‘·······，···‘···，··“···，，，，···，·········，，，，·”··中”，····，···”····““，·”二 1 q ‘ 引用标准 .··一 1 ︹口方法概要 .·1 乙仪器 .·1 巴口流动相 .·3 心 U 柱填充剂 ·································，，，·········，·，·········，”··········，，································，，，·… 6 2 月试验前的准备工作 .·一· ，····……，··········.··..·...·..·……9 匕卜操作 ······，··… 0 1 矽 0 色谱柱的评价 0 l 10 色谱图的整理 ··················································“······················“···············… … 11 11 定性分析 ················”···············，··········，···········”·················，，·”·················…… n 12 定量分析 ·一· 11 13 分子量的测定 ··············，····“·································.·，····································“…… 11 附录A(提示的附录) 用于液相色谱法中溶剂的性质 ······，·····，，，····‘···，，············”·······，·… 13 附录B(提示的附录)二元溶剂体系的组成与其强度的关系 ·······”·······················”··”····一 15 附录C(提示的附录)溶剂的选择性三角坐标 ························································…·… 16 附录D提示的附录) 离子交换色谱法中常用的缓冲剂 .·17 附录E(提示的附录)柱填充剂 ·································”·.，，··，···················.··..·...·..·.·.……18 附录F(提示的附录) 化学键合相柱填充剂 ······，·····“············.，·”·········，····”··············…… 19 附录G(提示的附录)环境要求 .·21 附录H(提示的附录)安全要求 ·············。”················”·············”·······”··········“······…·…21 附录J(提示的附录)典型标准色谱图的操

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