《荧光增白剂5BM的合成研究》-毕业论文设计（学术）.docVIP

荧光增白剂5BM的合成 PAGE PAGE 27 荧光增白剂5BM的合成 PAGE 1 XX 大 学 毕 业 论 文 题 目：荧光增白剂5BM的合成 学 号：X 姓 名：X 年 级：X 学 院：材料与化工学院 专 业：化学工程与工艺 指导教师：X 完成日期：X 摘 要 本文对国内外的荧光增白剂的研究现状以及今后的应用前景进行了讨论。研究了荧光增白剂5BM的合成路线，通过对产物的质量和收率进行分析寻找了最佳的合成条件。 荧光增白剂5BM主要应用于洗发液、洗手液、香皂、洗衣皂等日化产品当中，具有增白强度高、柔和性好、应用性能良好等优点。该品种在国内尚未生产，有很好的市场前景。 合成荧光增白剂5BM的主要原料有三聚氯氰、DSD酸、苯胺、尿素、氨水、N-甲基乙醇胺等试剂。以三聚氯氰为起始物经过三步缩合、酸析、抽滤、烘干几个过程最终获得产品，经过液相色谱实验分析产品纯度，用VBL作为标准样品获得产品相对的白度、甘白以及计算收率。 关键词：DSD酸；荧光增白剂；5BM；合成 Abstract The progress and application prospect of fluorescent whitening agents in the world and internal were discussed in this paper. The method to synthesize 5BM was researched and the best condition of the complex was studies by analyzing quality and yield coefficient. The fluorescent whitening agents 5BM is mainly used in Daily Chemical Products such as shampoo, liquid soap, perfumed soap, washing soap Etc. It has many advantages like, high whitening-strength, high soft and well application performance. It hasn’t been produced in inland and has promising market. The main procedure of synthesizing 5BM includes cyan uric chloride, DSD acid, aniline, urea, ammonium hydroxide and N-methyl ethanolamine. The synthesis of 5BM by cyan uric chloride as starting material through 3 condensations, Precipitated by acid, filter and dry. The Pureness was analyzed by High performance liquid chromatography. The fluorescent strength, whiteness and Gantz whiteness were tested using VBL as standard and the yields were calculated. Keyword: DSD acid; fluorescent whitening agents; 5BM; synthesize 目 录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc262383135 1 文献综述 PAGEREF _Toc262383135 \h 1 HYPERLINK \l _Toc262383136 1.1 荧光增白剂的定义和作用 PAGEREF _Toc262383136 \h 1 HYPERLINK \l _Toc262383137 1.2荧光增白剂的增白机理 PAGEREF _Toc262383137 \h